Environment-friendly tea feed containing black tea, dark tea, bamboo leaf and hawthorn
An environmentally friendly and green technology, used in animal feed, animal feed, applications, etc.
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Embodiment 1
[0084] Extract 20 kg of black tea, 30 kg of Fuzhuan black tea, 30 kg of bamboo leaves, and 2 kg of hawthorn, dry, pulverize, sieve to 80 mesh, distill and extract twice, and concentrate the extract in centrifugal vacuum to obtain a concentrate. Add ethanol to the concentrate to precipitate. The optimized process is leaching solvent 75% ethanol, material-to-liquid ratio 1:60 (g / mL), temperature 70°C, degree of fragmentation 80 mesh, leaching stages 2, leaching time 2 hours for 1st stage, and leaching time for 2nd stage After 0.5h, the extraction rate was 35.98%. The obtained precipitate was washed with absolute ethanol, anhydrous ether and acetone in turn, and then sent into a vacuum crystallizer. The pressure drops and the solution boils and cools down. Adjust the pumping rate of the vacuum system to reduce the pressure and temperature in the device according to the predetermined level until it reaches the predetermined level. Keep the solution in the crystallizer circulatin...
Embodiment 2
[0086] Extract 2 kg of black tea, 3 kg of Fuzhuan black tea, 3 kg of bamboo leaves, and 2 kg of hawthorn, dry, pulverize, sieve to 80 mesh, distill and extract twice, and concentrate the extract in a centrifugal vacuum to obtain a concentrate. Add ethanol to the concentrate to precipitate. The optimized process is leaching solvent 75% ethanol, material-to-liquid ratio 1:60 (g / mL), temperature 70°C, degree of fragmentation 80 mesh, leaching stages 2, leaching time 2 hours for 1st stage, and leaching time for 2nd stage 0.5h, the extraction rate was 35.98%. The obtained precipitate was washed with absolute ethanol, anhydrous ether and acetone in sequence, and then sent into a vacuum crystallizer. When the solution reached the specified level, the agitator and vacuum system were started to make the internal The pressure drops and the solution boils and cools down. Adjust the pumping rate of the vacuum system to reduce the pressure and temperature in the device according to the pr...
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