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Method for preparing titanium monoxide powder material

A powder material, titanium monoxide technology, applied in the direction of titanium oxide/hydroxide, etc., can solve the problems of harsh reaction conditions, residual titanium dioxide, and inability to obtain titanium monoxide, etc., and achieve the effect of simplifying the preparation process and improving the purity of the product

Inactive Publication Date: 2012-06-20
GUIZHOU BRANCH CHINA ALUMINUM IND
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  • Abstract
  • Description
  • Claims
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AI Technical Summary

Problems solved by technology

Among them, the reaction conditions of the magnesium reduction titanium dioxide method and the carbon reduction titanium dioxide method are relatively harsh, and the oxygen content is not easy to control; And the limitation of stoichiometric ratio, it is easy to cause the surplus of titanium or titanium dioxide, so that high-purity titanium monoxide cannot be obtained

Method used

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  • Method for preparing titanium monoxide powder material
  • Method for preparing titanium monoxide powder material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Weigh 960g mole of titanium dioxide powder, put it into a high-temperature furnace, pass 22g of hydrogen into the furnace, and sinter at 1200°C for 4 hours to successfully prepare high-purity titanium monoxide with a purity of 99.95%.

Embodiment 2

[0015] Weigh 960g mole of titanium dioxide powder, put it into a high-temperature furnace, pass 30g of hydrogen into the furnace, and sinter at 1800°C for 12 hours to successfully prepare high-purity titanium monoxide with a purity of 99.94%.

Embodiment 3

[0017] Weigh 960g mole of titanium dioxide powder, put it into a high-temperature furnace, pass 40g of hydrogen into the furnace, and sinter at 2000°C for 20 hours to successfully prepare high-purity titanium monoxide with a purity of 99.96%.

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Abstract

A method for preparing titanium monoxide powder materials relates to a method for preparing high-purity titanium monoxide powder materials through adopting a thermal reduction method, particularly to a method for preparing high-purity titanium monoxide powder materials. The method is characterized in that dititanium trioxide and high-purity hydrogen are taken as basic materials to carry out the high-temperature thermal reduction reaction. In the invention, hydrogen and dititanium trioxide are reduced to titanium monoxide at a high temperature through changing base materials (namely, replacing titanium dioxide with dititanium trioxide), so that the high-purity titanium monoxide is obtained.

Description

technical field [0001] The invention discloses a method for preparing titanium monoxide powder material, which relates to the preparation of high-purity titanium monoxide powder material by thermal reduction method, especially the preparation method of high-purity titanium monoxide powder material. Background technique [0002] Titanium monoxide and gold belong to the same face-centered cubic crystal system, and its color is closest to the color of gold in nature, so titanium monoxide can be used in the decoration industry and related fields. In addition, titanium monoxide can be used as a catalyst for ethylene polymer reactions and is widely used in the semiconductor industry. [0003] At present, the preparation methods of titanium monoxide mainly include magnesium reduction titanium dioxide method under hydrogen atmosphere, hydrogen reduction titanium dioxide method under hydrogen atmosphere, carbon reduction titanium dioxide method, and titanium reduction titanium dioxid...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01G23/04
Inventor 秦庆东王芳平邱仕麟柴登鹏
Owner GUIZHOU BRANCH CHINA ALUMINUM IND
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