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Wear-resistant crystallized glass plate and preparation method thereof

A glass-ceramic and plate technology, which is applied in the field of industrial wear-resistant plates, can solve the problems of poor product color and aesthetics, insignificant production cost, and failed to be successfully promoted, so as to solve the problems of poor color and aesthetics, The surface is soft and crystal clear, and the effect of reducing production costs

Inactive Publication Date: 2014-01-29
水经(上海)生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The energy consumption of this process is relatively high. Compared with the production process of pure material glass ceramics, it has no obvious advantages in production cost. At the same time, the prepared products are poor in color and aesthetics. This process of crystal glass has not been successfully promoted.

Method used

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  • Wear-resistant crystallized glass plate and preparation method thereof
  • Wear-resistant crystallized glass plate and preparation method thereof
  • Wear-resistant crystallized glass plate and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] process such as figure 1 As shown, the specific steps are:

[0034] Crushing and screening steel slag and quartz sand;

[0035] The raw material components are weighed and mixed according to the proportion by weight; specifically: 65 parts of iron and steel slag, 20 parts of quartz sand, 6 parts of magnesium oxide, 5 parts of titanium dioxide, and 1 part of calcium fluoride.

[0036] The composition and weight percent content of the iron and steel slag are: SiO 2 15%, FeO 15%, CaO 50%, MgO5%, Al 2 o 3 2%, TFe 10%, MnO 2%, P 2 o 3 0.5%, MFe 0.5%.

[0037] Place the above raw material components in a crucible kiln and melt at 1380°C for 3 hours; after the melting is completed, pour the molten glass directly into water and quench it into glass pellets (the viscosity of the molten glass is 10Pa.s, the nucleation temperature is 735°C, and the nucleation time 1h); spread the glass granules in a refractory abrasive tool and carry out crystallization in a shuttle kiln...

Embodiment 2

[0039] process such as figure 1 As shown, the specific steps are:

[0040] Crushing and screening steel slag and quartz sand;

[0041] The raw material components are weighed and mixed according to the proportion by weight; specifically: 85 parts of iron and steel slag, 30 parts of quartz sand, 10 parts of magnesium oxide, 10 parts of titanium dioxide, and 3 parts of calcium fluoride.

[0042] The composition and weight percent content of the iron and steel slag are: SiO 2 20%, FeO 10%, CaO 40%, MgO5%, Al 2 o 3 5%, TFe 15%, MnO 4%, P 2 o 3 0.1%, MFe 0.9%.

[0043] Place the above raw material components in a crucible kiln and melt at 1450°C for 1 hour; after the melting is completed, pour the molten glass directly into water and quench it into glass pellets (the viscosity of the molten glass is 12Pa.s, the nucleation temperature is 710°C, and the nucleation time 2h); spread the glass granules in a refractory abrasive tool for crystallization in a box-type electric fu...

Embodiment 3

[0045] process such as figure 1 As shown, the specific steps are:

[0046] Crushing and screening steel slag and quartz sand;

[0047] The raw material components are weighed and mixed according to the proportion by weight; specifically: 70 parts of iron and steel slag, 25 parts of quartz sand, 8 parts of magnesium oxide, 7.5 parts of titanium dioxide, and 2 parts of calcium fluoride.

[0048] The composition and weight percent content of the iron and steel slag are: SiO 2 15%, FeO 10%, CaO 40%, MgO 10%, Al 2 o 32%, TFe 20%, MnO 2%, P 2 o 3 0.3%, MFe 0.7%.

[0049] Place the above raw material components in a crucible kiln and melt at 1400°C for 2.2 hours; after the melting is completed, pour the molten glass directly into water and quench it into glass pellets (the viscosity of the molten glass is 11.5Pa.s, and the nucleation temperature is 715°C, forming The nuclear time is 1.2h); the glass granules are spread flat in the refractory abrasive tool and crystallized in...

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Abstract

The invention discloses a wear-resistant crystallized glass plate and a preparation method thereof. The wear-resistant crystallized glass plate consists of the following components in parts by weight: 65-85 parts of steel and iron furnace slag, 20-30 parts of quartz sand, 6-10 parts of magnesium oxide, 5-10 parts of titanium dioxide and 1-3 parts of calcium fluoride, wherein the steel and iron furnace slag comprises the following components in percentage by weight: 13-20 percent of SiO2, 10-15 percent of FeO, 40-50 percent of CaO, 5-10 percent of MgO, 2-5 percent of Al2O3, 10-20 percent of TFe, 2-5 percent of MnO2, 0.1-0.5 percent of P2O3 and 0.5-1.5 percent of MFe. The method comprises burdening, melting, water quenching, grinding, sieving, press molding, nucleating, crystallizing and rubbing down, wherein melting is performed at the temperature of 1,380-1,450 DEG C for 1-3 hours; and crystallizing is performed at the temperature of 900-920 DEG C for 1-2 hours. Compared with the prior art, the wear-resistant crystallized glass plate has the advantages of low raw material cost, excellent melting performance, excellent crystallizabitity, high plate hardness, high bending strength, soft and bright surface gloss, denseness, immaculacy and wide product market prospect.

Description

technical field [0001] The invention relates to the technical field of industrial wear-resistant plates, in particular to a wear-resistant glass-ceramic plate and a preparation method thereof. Background technique [0002] Glass-ceramics (Glass-Ceramics), also known as glass-ceramics or micro-ceramic ceramics, is a kind of glass-ceramics containing a large number of micro-crystals, which is obtained by adding a crystal nucleating agent and undergoing certain heat treatment conditions to control the crystallization of glass. polycrystalline solid material. The structure and properties of glass-ceramic are different from ceramics and glass, and its properties depend on the mineral composition and microstructure of the microcrystalline ceramic phase and the chemical composition of glass, so it combines the characteristics of ceramics and glass and has low thermal expansion Coefficient, high mechanical strength, remarkable corrosion resistance, weathering resistance and good th...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C10/12
Inventor 易明
Owner 水经(上海)生物科技有限公司
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