Organic/inorganic wire enamel and preparation method thereof
An enameled wire enamel and inorganic technology, applied in the field of enamelled wire enamel, can solve the problems of expensive solvent, high cost of polyimide and polyamideimide, and achieve the effect of simple preparation method, good freeze resistance and low cost
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Embodiment 1
[0019] Embodiment 1: Organic-inorganic wire enamelled varnish, the parts by weight of its constituent raw materials are: 110 parts of xylenol, 100 parts of trimellitic anhydride, 100 parts of maleic anhydride, 30 parts of diaminodiphenylmethane, 30 parts of acrylate, glycerin 15 parts, 40 parts of neopentyl glycol, 40 parts of dimethyl terephthalate, 1 part of straw ash, 2 parts of tetrabutoxytitanium, 1 part of attapulgite, 1 part of N-methylpyrrolidone, 3 parts of phenolic resin %.
Embodiment 2
[0020] Embodiment 2: organic-inorganic wire enamelled varnish, the parts by weight of its raw materials are: 115 parts of xylenol, 105 parts of trimellitic anhydride, 102 parts of maleic anhydride, 35 parts of diaminodiphenylmethane, 35 parts of acrylate, glycerin 18 parts, neopentyl glycol 45 parts, dimethyl terephthalate 45 parts, straw ash 2 parts, tetrabutoxytitanium 3 parts, attapulgite 2 parts, N-methylpyrrolidone 1.5 parts, amino resin 2 parts %.
Embodiment 3
[0021] Embodiment 3: Organic-inorganic wire enamelled varnish, the parts by weight of its raw materials are: 120 parts of xylenol, 110 parts of trimellitic anhydride, 105 parts of maleic anhydride, 40 parts of diaminodiphenylmethane, 40 parts of acrylate, glycerin 20 parts, neopentyl glycol 50 parts, dimethyl terephthalate 50 parts, straw ash 3 parts, tetrabutoxytitanium 5 parts, attapulgite 3 parts, N-methylpyrrolidone 2 parts, amino resin 3 parts %.
[0022] The preparation method of organic-inorganic wire enamel of the present invention comprises the following steps:
[0023] (1) Add trimellitic anhydride, maleic anhydride, dimethyl terephthalate and acrylic acid ester into the reaction kettle according to the weight of the raw materials, heat to 150-200°C, and react for 4.5-5.5 hours;
[0024] (2) Add diaminodiphenylmethane to the solution obtained in step (1) by weight, keep it at 155-180°C, and keep it warm for half an hour;
[0025] (3) Add neopentyl glycol and glycer...
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