Method and equipment for measuring total solid matter content of natural rubber latex
A technology of natural rubber latex and total solids, applied in the field of natural rubber, can solve the problems of time-consuming, cumbersome operation, power consumption, etc., and achieve the effect of expanding the area, high measurement accuracy and convenient operation
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Embodiment 1
[0029] Example 1: Operation method
[0030] 1. Use a disposable syringe to drop a small amount of latex sample into a numbered container of rated weight (including foam metal with a weight of ω 0 ), weigh the total weight ω of the sample and the vessel 1 , prepare several samples to be determined according to this method;
[0031] 2. Place the prepared vessel on the heat source in the vacuum system, turn on the vacuum switch, and make the system reach a negative pressure state.
[0032] 3. Use the temperature controller to set the heating temperature to 180-350°C, set a few minutes, and vacuum dry the sample;
[0033] 4. Weigh and measure the dried sample together with the vessel to obtain the weight ω 2 ;Use the following formula to calculate the total solid content α of the sample:
[0034] .
Embodiment 2
[0036] A kind of measuring equipment of the total solid content of natural rubber latex, comprise the metal container 6 that is made of metal foam of rated weight, the electric heating plate 5 of heating metal container 6, described measuring equipment also includes the described metal container 6. A sealed box 1 for vacuuming. The measuring equipment also includes temperature, vacuum and other function control knobs 3. The temperature, vacuum and other function control knobs 3 control the electric heating plate 5 and the vacuum pump 2. Control, the measuring device also includes a plate weighing system 4, and the measuring device also includes a digital display 7. The metal foam is covered with metal foil 8 on its side and bottom.
[0037]
Embodiment 3
[0039] The samples were fresh natural rubber latex purchased from the purchase point of the rubber factory on the same day.
[0040] 1. Determination of total solids content by standard oven drying method: use a disposable syringe to take 2 to 3 grams of latex for determination, drying temperature is 70 ° C, time is 10 hours, and three groups of sample tests are done;
[0041] ω 0 : vessel weight;
[0042] ω 1 : The total weight of the container and latex before measurement;
[0043] ω2 : The total weight of the container and latex after drying;
[0044]
[0045] 2. Determination of total solids content by vacuum drying method (using the method of Example 1 and the equipment of Example 2): use a disposable syringe, take 0.2 to 2 grams of latex for measurement, drying temperature 200 ° C, vacuum degree -0.09 Mpa, time 3 minutes, do three sets of sample tests;
[0046] ω 0 : vessel weight;
[0047] ω 1 : The total weight of the container and latex before measurement; ...
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