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Detection method for sea dragon and gecko oral liquid

A sea dragon gecko oral solution and a technology for gecko oral solution, which are applied in the detection field of sea dragon gecko oral solution, can solve the problems of comprehensive control and detection, can not guarantee the quality of medicines, and have few inspection items, and can increase the number of indications and increase the efficiency. The effect of liquid chromatography on content determination and advanced detection methods

Active Publication Date: 2012-07-25
山东宏济堂制药集团股份有限公司
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  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the original standard, only the TLC identification of the medicinal materials ginseng and scutellaria baicalensis, because the original standard has few testing items and a single method, it cannot guarantee the comprehensive control and testing of the quality of the drug

Method used

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  • Detection method for sea dragon and gecko oral liquid
  • Detection method for sea dragon and gecko oral liquid
  • Detection method for sea dragon and gecko oral liquid

Examples

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Effect test

Embodiment 1

[0035]Take 39.1g of sea dragon, 0.73g of gecko, 4.68g of ginseng, 4.68g of sheep penis, 4.68g of sheep kidney, 4.68g of scutellaria baicalensis, 3.1g of rehmannia glutinosa, 3.1g of dodder seed, 3.1g of Polygonum multiflorum, 3.1g of rehmannia glutinosa, 3.1g of tangerine peel, and angelica 1.56g, astragalus 4.68g, actinolite 1.56g, lotus root 1.56g, licorice 1.56g, chuanxiong 1.56g, alisma 1.56g, Cynomorium 1.56g, cardamom 1.56g, agarwood 1.56g, antler 1.56g, medlar 1.56g, 0.78g of Cistanche, 1.56g of Epimedium (burned with sheep oil), 1.56g of cinnamon, 1.56g of leek seed, 1.56g of Cnidium, 0.31g of Zanthoxylum bungeanum, add water and decoct twice, each time for 2 hours , combine the decoctions, concentrate at 80°C to a clear paste with a relative density of 1.04-1.06, add twice the amount of ethanol, refrigerate for 12 hours, filter, concentrate, add water, refrigerate, filter, add an appropriate amount of benzoic acid to the filtrate to dissolve, Use 8% sodium hydroxide t...

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Abstract

The invention discloses a quality control and detection method for a sea dragon and gecko oral liquid. In the quality control and detection method, on the basis of the original detection standard, a thin-layer chromatography detection method for dried tangerine or orange peel and astragalus root in the prescription of the sea dragon and gecko oral liquid is added, a thin-layer chromatography for ginseng and the astragalus root is improved, and a high performance liquid chromatography for measuring the content of epimedim herb of in the prescription is added. The detection project designed by the invention is reasonable; and the detection method provided by the invention has the advantages of advancement and good accuracy and repeatability, is used for carrying out the quality control on the sea dragon and gecko oral liquid, and can carry out the comprehensive quality control on the sea dragon and gecko oral liquid to ensure the stability and uniformity of product quality.

Description

technical field [0001] The invention discloses a method for detecting the gecko oral liquid with the functions of warming the kidney and strengthening yang, and nourishing essence and blood. Background technique [0002] "Hailong Gecko Oral Liquid" functions and indications: warming kidney and strengthening yang, nourishing essence and blood. For soreness and weakness of the waist and feet, pale complexion, impotence and nocturnal emission, cold uterine infertility, dizziness in the head. [0003] The original test standard of "Hailong Gecko Oral Liquid" is recorded in the Thirteenth Volume of Chinese Medicine Prescriptions in Drug Standards of the Ministry of Health of the People's Republic of China. In the original standard, only the TLC identification of the medicinal materials ginseng and scutellaria baicalensis was carried out. Since the original standard had few testing items and a single method, it could not guarantee the comprehensive control and testing of the qual...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/36A61K33/26A61K35/32A61K35/48A61K35/56A61K35/583A61K35/60
Inventor 李樱刘圣梅姜广玲秦秀玲
Owner 山东宏济堂制药集团股份有限公司
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