Method for detecting multiple allergic aroma agents in toys
A detection method and allergy technology, applied in the fields of toy safety and analytical chemistry, can solve the problems of not covering allergic flavors, not forming a system, etc., to shorten the detection process, reduce the sample volume, and improve the analysis efficiency.
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Embodiment 1
[0028] Sample preparation and determination methods for 45 allergic fragrances in soap for children:
[0029] (1) Extraction:
[0030] Accurately weigh 22.15mg (accurate to 0.01mg) of the sample, put it into the quartz tube of the sample heat treatment instrument with clean stainless steel tweezers, then insert the adsorption tube loaded with adsorbent into the sample heat treatment instrument, turn on the carrier gas, and the flow rate is 300mL / min. Set the temperature at 55°C, process the sample for 5 minutes, then rapidly raise the temperature to 70°C, keep it for another 5 minutes, and finally raise the temperature rapidly to 85°C, and keep it for 10 minutes. Then put the adsorption tube into the thermal desorption autosampler for testing. The method parameters used are shown in Table 1 and Table 2 respectively:
[0031] Table 1 Conditions of thermal desorption device
[0032] split mode
splitless
The initial temperature
30℃
0...
Embodiment 2
[0050] Sample preparation and determination methods for 45 allergic fragrances in plush toys:
[0051] (1) Extraction:
[0052] Accurately weigh 20.32mg (accurate to 0.01mg) powder plush, put it into the quartz tube of the sample heat treatment instrument with clean stainless steel tweezers, then insert the adsorption tube loaded with adsorbent into the sample heat treatment instrument, turn on the carrier gas, flow rate It is 330mL / min. Set the temperature to 55°C, process the sample for 7 minutes, rapidly raise the temperature to 70°C, keep it for another 7 minutes, and finally raise the temperature rapidly to 85°C, and keep it for 15 minutes. Then put the adsorption tube into the thermal desorption autosampler for testing. The method parameters used are shown in Table 1 and Table 2 respectively:
[0053] Table 1 Conditions of thermal desorption device
[0054] split mode
splitless
The initial temperature
35℃
0.5 minutes
h...
Embodiment 3
[0064] Sample preparation and determination methods for 45 allergic fragrances in plastic toys:
[0065] (1) Extraction:
[0066] Accurately weigh 22.89mg (accurate to 0.01mg) of blue plastic, put it into the quartz tube of the sample heat treatment instrument with clean stainless steel tweezers, then insert the adsorption tube loaded with adsorbent into the sample heat treatment instrument, turn on the carrier gas, flow rate It is 320mL / min. Set the temperature to 55°C, process the sample for 6 minutes, rapidly raise the temperature to 70°C, and keep it for another 6 minutes, and finally raise the temperature rapidly to 85°C, and keep it for 12 minutes. Then put the adsorption tube into the thermal desorption autosampler for testing. The method parameters used are shown in Table 1 and Table 2 respectively:
[0067] Table 1 Conditions of thermal desorption device
[0068] split mode
splitless
The initial temperature
32℃
0.4 minutes...
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