Material for rapid three dimensional printing forming and preparation method thereof
A technology for three-dimensional printing and forming materials, applied in the field of materials for three-dimensional printing rapid prototyping and its preparation, can solve the problems that restrict the promotion and popularization of 3DP forming technology, the forming accuracy of small parts is not high enough, and the adhesive bonding is not strong enough, etc. problem, to achieve the effect of short bonding time, good compounding effect and optional color.
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Embodiment 1
[0033] In the first step, 1 kilogram of magnesium silicate and 5 kilograms of acetone are added to a grinder with a rotating speed of 5000 rpm, and ground for 1 hour;
[0034] In the second step, 1 gram of Span-60, 2 grams of octadecanoic acid, and 50 grams of polyacrylic acid were added to 1 kilogram of acetone and stirred and dispersed for 2 hours to obtain a modified solution;
[0035] The third step is to mix the powder material pretreatment material obtained in the first step with the modified liquid obtained in the second step, put it into a grinder, mix and grind at room temperature for 4 hours, and then carry out supercritical drying, and grind and pulverize the dried material. The modified powder material A is obtained, and the particle size of the product is 700nm.
Embodiment 2
[0037] In the first step, 0.4 kg of sodium sulfate, 0.6 kg of calcium phosphate, 1 kg of ethanol, and 9 kg of glycerin were added to a grinder at a speed of 6000 rpm, and grinded for 2 hours;
[0038] In the second step, 10 grams of polyoxyethylene ether, 1 gram of sodium sulfonate, and 100 grams of polymethyl acrylate were added to 5 kilograms of ethanol and stirred and dispersed for 3 hours to obtain a modified solution;
[0039] The third step is to mix the powder material pretreatment material obtained in the first step with the modified liquid obtained in the second step, put it into a grinder, mix and grind at room temperature for 10 hours, and then carry out supercritical drying, and grind and pulverize the dried material. The modified powder material A is obtained, and the particle size of the product is 900nm.
Embodiment 3
[0041] In the first step, 0.7 kg of calcium sulfate, 0.5 kg of calcium silicate, 0.1 kg of calcium phosphate and 2 kg of isobutanol are added to a grinder with a rotation speed of 5500 rpm, and grind for 1.5 hours;
[0042]In the second step, 20 grams of sodium dodecylbenzenesulfonate, 15 grams of sodium sulfonate, and 100 grams of polyethylene glycol were added to 2.8 kilograms of ethanol and 0.2 kilograms of dibutyl phthalate and stirred and dispersed for 2.5 hours to obtain the modified Sexual fluid;
[0043] The third step is to mix the powder material pretreatment material obtained in the first step with the modified liquid obtained in the second step, put it into a grinder, mix and grind at room temperature for 8 hours, and then carry out supercritical drying, and grind and pulverize the dried material. The modified powder material A is obtained, and the particle size of the product is 1000nm.
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