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Mugwort leaf oil microcapsule antibacterial crease-resistant fabric and preparation method thereof

A technology of mugwort oil and microcapsules, applied in the directions of plant fibers, textiles and papermaking, fiber processing, etc., can solve the problems of huge investment in blended spinning equipment, has not been promoted on a large scale, and high technical content, and achieve excellent health care functions and appearance. Good shape and the effect of promoting blood circulation

Active Publication Date: 2011-05-18
THE HONG KONG POLYTECHNIC UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, blended spinning has huge investment equipment and high technical content, and has not yet been widely promoted.

Method used

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  • Mugwort leaf oil microcapsule antibacterial crease-resistant fabric and preparation method thereof
  • Mugwort leaf oil microcapsule antibacterial crease-resistant fabric and preparation method thereof
  • Mugwort leaf oil microcapsule antibacterial crease-resistant fabric and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0053] (1) Emulsification of mugwort oil: Weigh 0.50g of gelatin and 0.50g of gum arabic into a 250mL three-necked flask, add 100mL of distilled water, install a mechanical stirrer, stir and dissolve in a water bath at 40°C, and prepare gelatin-arabic The mixed solution of the glue system has a concentration of 0.5% (W / V), and then adds 1.0mL mugwort oil, and emulsifies for 10 minutes at a stirring speed of 800 rpm;

[0054] (2) Complex coagulation reaction: keep the stirring speed and water bath temperature constant during emulsification, gradually add 10% HAC solution dropwise to the above emulsion to adjust the pH value of the system to 4.0, reduce the stirring speed to 300 rpm, remove Water bath, continue to stir at room temperature for 10 minutes;

[0055] (3) Cross-linking and solidification: cool the above-mentioned coagulated microcapsule suspension to 0-5° C. in an ice-water bath for 30 minutes, then adjust the pH value of the system to 7.0 with 10% NaOH solution, add...

Embodiment 2

[0061] (1) Emulsification of mugwort oil: Weigh 1.00g gelatin and 1.00g gum arabic into a 250mL three-necked flask, add 100mL distilled water, install a mechanical stirrer, stir and dissolve in a water bath at 40°C, add 1.0mL mugwort oil , emulsifying for 15 minutes at a stirring speed of 800 rpm;

[0062] (2) Complex coagulation reaction: keep the stirring speed and water bath temperature constant during emulsification, gradually add 10% HAC solution dropwise to the above emulsion to adjust the pH value of the system to 4.0, reduce the stirring speed to 250 rpm, remove Water bath, continue to stir at room temperature for 10 minutes;

[0063] (3) Cross-linking solidification: Cool the above-mentioned condensed suspension to 0-5°C in an ice-water bath for 30 minutes, then adjust the pH value of the system to 7.0 with 10% NaOH solution, add 4 mL of 25% glutaraldehyde solution dropwise, and stir Continue the ice bath for 30 minutes at a speed of 300 rpm; move to a water bath at ...

Embodiment 3

[0069] (1) Emulsification of mugwort oil: Weigh 5.00g of gelatin and 5.00g of gum arabic into a 250mL three-necked flask, add 100mL of distilled water, install a mechanical stirrer, stir and dissolve in a water bath at 40°C, add 5.0mL of mugwort oil , emulsified for 20 minutes at a stirring speed of 1000 rpm.

[0070] (2) Coagulation reaction: Keep the stirring speed and water bath temperature constant during emulsification, gradually add 10% HAC solution dropwise to the above emulsion to adjust the pH value of the system to 4.0, reduce the stirring speed to 600 rpm, and remove from the water bath , continue stirring at room temperature for 10 minutes;

[0071] (3) Cross-linking solidification: Cool the above-mentioned condensed suspension to 0-5°C in an ice-water bath for 30 minutes, then adjust the pH value of the system to 7.0 with 10% NaOH solution, add 10 mL of 25% glutaraldehyde solution dropwise, and stir Continue the ice bath for 30 minutes at a speed of 350 rpm; move...

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Abstract

The invention relates to a method for preparing a mugwort leaf oil microcapsule antibacterial crease-resistant fabric. The method comprises the following steps of: 1) emulsifying mugwort leaf oil in an emulsifying agent made of wall material; 2) performing complex coagulation reaction on the emulsified mugwort leaf oil; 3) cross-linking and curing the emulsion after the complex coagulation reaction to obtain mugwort leaf oil microcapsule emulsion; 4) adding crease-resistant cross linker, catalyst and penetrating agent into the obtained mugwort leaf oil microcapsule emulsion to prepare a mugwort leaf oil microcapsule antibacterial crease-resistant fabric finishing agent; and 5) treating the fabric by using the prepared mugwort leaf oil microcapsule antibacterial crease-resistant fabric finishing agent to obtain the mugwort leaf oil microcapsule antibacterial crease-resistant fabric. The invention also relates to the mugwort leaf oil microcapsule antibacterial crease-resistant fabric prepared by using the method. The mugwort leaf oil microcapsule antibacterial fabric has antibacterial and anti-inflammatory functions, meanwhile has crease-resistant and ironing-free functions, and has good washing fastness.

Description

technical field [0001] The invention relates to an antibacterial and anti-wrinkle fabric with mugwort leaf oil microcapsules and a preparation method thereof. Background technique [0002] A microencapsule is a semipermeable or hermetically sealed microcapsule with a polymer wall that can embed and protect certain substances. Microcapsule technology is the use of natural or synthetic polymer materials (usually called wall materials) to encapsulate dispersed solid material particles, liquid droplets or gases (usually called core materials) in a film to form tiny capsules. A technology whose diameter is generally 1 to 1000 μm. Microcapsules have many unique functions, such as protecting the core material from the environment, reducing toxicity, masking bad taste, controlling the release of the core material, prolonging the efficacy, prolonging the storage period, changing the physical state for easy portability and transportation, and changing physical properties to make it e...

Claims

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Application Information

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IPC IPC(8): D06M23/12D06M15/39D06M13/192D06M101/06
CPCD06M2200/20D06M23/12
Inventor 李鹂区伟文汪国成钟慧仪李毅
Owner THE HONG KONG POLYTECHNIC UNIV
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