Drainage phase-change temperature-regulation heat-insulation coating and preparation method thereof
A technology of thermal insulation coatings and phase change materials, applied in the direction of polyether coatings, polyurea/polyurethane coatings, coatings, etc., can solve the problems of immature thermal insulation coatings and unfavorable environmental protection
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[0047] The present invention also designs a preparation method (referred to as the preparation method) of the water-based phase-change temperature-regulating heat-insulating coating. The preparation method is based on the coating of the material in parts by weight in the present invention, and includes three steps of preparing component A, component B and finally preparing the heat-insulating coating. The preparation method of the present invention adopts following technology:
[0048] 1 Preparation of component A At room temperature, according to the composition of component A by weight, first add the JFC, sodium dodecylsulfonate, and OP-10 to deionized water for stirring, and then add polyethylene Diol 800 and polyethylene glycol 1000, put the solution in a water bath at a temperature of 55-75°C, stir evenly, after the polyethylene glycol is completely dissolved, add 52# paraffin, stir slowly, and wait until the paraffin is completely melted, At the speed of 1500-3000r / min,...
Embodiment 1
[0054] Preparation of Component 1A
[0055] At room temperature, phase-change functional fillers were prepared in parts by mass. Add 0.1 parts of JFC, 0.3 parts of sodium dodecylsulfonate and 0.1 parts of OP-10 to 40 parts of deionized water, stir well, and put the solution in 60 In a water bath at ℃, add 5 parts of polyethylene glycol 800 and 1 part of polyethylene glycol 1000, stir to dissolve them all, then add 1 part of 52# paraffin, after the paraffin is completely melted, at a speed of 1500r / min, Perform high-speed stirring and emulsification to obtain a uniform emulsion. At 100r / min, stir slowly, add 15 parts of expanded perlite and 5 parts of diatomaceous earth in sequence, stir for 30 minutes, and cool to room temperature to obtain a phase-change functional filler (Group A points), ready for use;
[0056] Preparation of Component 2B
[0057] At room temperature, prepared according to the number of parts by mass, add 0.1 parts of S-6302 water-based film-forming aid a...
Embodiment 2
[0061] Preparation of Component 1A
[0062] At room temperature, prepare phase-change functional fillers according to the number of parts by mass. Add 0.2 parts of JFC, 0.4 parts of sodium dodecylsulfonate and 0.15 parts of OP-10 to 45 parts of deionized water, stir well, and put the solution in 65 In a water bath at ℃, add 10 parts of polyethylene glycol 800 and 3 parts of polyethylene glycol 1000, stir to dissolve them all, then add 3 parts of 52# paraffin, after the paraffin is completely melted, at a speed of 2000r / min, Perform high-speed stirring and emulsification to obtain a uniform emulsion. At 120r / min, stir slowly, add 25 parts of expanded perlite and 10 parts of diatomaceous earth in sequence, stir for 10 minutes, and cool to room temperature to obtain a phase-change functional filler (Group A points), ready for use;
[0063] Preparation of Component 2B
[0064] At room temperature, according to the mass parts, add 0.2 parts of S-6302 water-based film-forming addi...
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Abstract
Description
Claims
Application Information
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