Flame-retarded lubricating grease and preparation method thereof
A grease, flame-retardant technology, applied in the field of flame-retardant grease and its preparation, can solve the problems of easy blockage of pipelines, inability to solve the problems of self-ignition of grease by heat, lack of oil lubrication in machinery, etc., and achieves long service life and excellent mechanical properties. Stable, low cost effect
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Embodiment 1
[0029] Embodiment 1: The preparation method of a kind of flame-retardant lubricating grease of the present invention adopts the following process steps:
[0030] 1. Fatty acid calcium soap is formed by the reaction of lauryl hydroxystearic acid, calcium hydroxide and water:
[0031] Heat 180g of water to 90°C, add 16.8g of dodecyl hydroxystearic acid, add 2.1g of calcium hydroxide after the lauryl hydroxystearic acid is melted, saponify for 1 hour, stir evenly, take a sample and measure it with a phenolphthalein indicator to show a reddish color It is alkaline, keep it warm for 0.8 hours at 95°C, put it in a container to dry, and set it aside.
[0032] 2. Lithium fatty acid soap is generated by the reaction of lauryl hydroxystearic acid, lithium hydroxide and water:
[0033] Heat 650g of water to 90°C, add 100.8g of lauryl hydroxystearic acid, add 8.4g of lithium hydroxide after the lauryl hydroxystearic acid is melted, saponify for 1 hour, stir evenly, take samples and measu...
Embodiment 2
[0037] Embodiment two: the preparation method of a kind of flame-retardant lubricating grease of the present invention adopts following process step:
[0038] 1. Fatty acid calcium soap is formed by the reaction of lauryl hydroxystearic acid, calcium hydroxide and water:
[0039] Heat 118g of water to 95°C, add 10.5g of dodecyl hydroxystearic acid, add 1.3g of calcium hydroxide after the lauryl hydroxystearic acid is melted, saponify for 1.25 hours, stir evenly, take a sample and measure it with a phenolphthalein indicator to show a reddish color It is alkaline, keep it warm for 1 hour at a temperature of 100°C, put it in a container to dry, and set it aside.
[0040] 2. Lithium fatty acid soap is generated by the reaction of lauryl hydroxystearic acid, lithium hydroxide and water:
[0041] Heat 450g of water to 95°C, add 62.4g of dodecyl hydroxystearic acid, add 5.2g of lithium hydroxide after the lauryl hydroxystearic acid is melted, saponify for 1.25 hours, stir evenly, take...
example 3
[0045] Example three: the preparation method of a kind of flame-retardant lubricating grease of the present invention, adopts following process steps:
[0046] 1. Fatty acid calcium soap is formed by the reaction of lauryl hydroxystearic acid, calcium hydroxide and water:
[0047] Heat 75g of water to 100°C, add 7.6g of dodecyl hydroxystearic acid, add 0.95g of calcium hydroxide after the dodecyl hydroxystearic acid is melted, saponify for 1.5 hours, stir evenly, take a sample and measure it with a phenolphthalein indicator to show a reddish color It is alkaline, keep it warm for 1.2 hours at 105°C, put it in a container to dry, and set it aside.
[0048] 2. Lithium fatty acid soap is generated by the reaction of lauryl hydroxystearic acid, lithium hydroxide and water:
[0049] Heat 110g of water to 100°C, add 11.4g of lauryl hydroxystearic acid, add 3.8g of lithium hydroxide after the lauryl hydroxystearic acid is melted, saponify for 1.5 hours, stir evenly, and take samples...
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