Compound electret membrane, preparation method thereof and use thereof
An electret and polar film technology, applied in the field of composite electret film and its preparation, can solve problems such as no report of composite electret film, achieve simple and reliable technical equipment, mature electret method, and promote micro-electret. loop effect
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Embodiment 1
[0022] The preparation of embodiment 1 composite electret film
[0023] Take porous membrane PTFE (thickness about 160 μm, pore size 5 μm), FEP membrane (thickness about 50 μm, pore size 5 μm), and melt at 300°C for 20 minutes to prepare PTFE / FEP electret membrane. Electrode, needle voltage -12kv, room temperature electret 1min, prepared surface voltage -1kv. Store in a desiccator for later use.
[0024] Take 1g of dragon's blood fine powder and dissolve it with 100ml of ethanol to prepare a liquid with a concentration of 10mg / ml. Take a PP film (film thickness 13 μm, pore size 5 μm), soak it in the liquid medicine, take it out after 8 hours, and dry it under reduced pressure at 80°C to constant weight. The drug loading is 0.053mg / cm 2 .
[0025] The composite electret film was prepared by softening and melting the drug-loaded PP film and the PTFE / FEP electret film at 120°C.
Embodiment 2
[0026] The preparation of embodiment 2 composite electret film
[0027] Take porous membrane PTFE (film thickness about 160 μm, pore diameter 5 μm), FEP membrane (film thickness about 50 μm, pore diameter 5 μm), melt at 300 ° C for 20 minutes, prepare PTFE / FEP electret membrane, and use constant voltage negative corona electret for the surface , needle voltage -12kv, room temperature electret 1min, prepared surface voltage -1kv. Store in a desiccator for later use.
[0028] Take 30g of notoginseng fine powder, extract with 300ml of ethanol under reflux, and extract 3 times, each time for 1h. The extracts were combined and concentrated, evaporated to dryness under reduced pressure, weighed 1 g of the dried product, and dissolved it in 100 ml of ethanol to prepare a drug solution with a concentration of 10 mg / ml. Take a PP film (film thickness 13 μm, pore size 5 μm), soak it in the liquid medicine, take it out after 8 hours, and dry it under reduced pressure at 80°C to constan...
Embodiment 3
[0030] The preparation of embodiment 3 composite electret film
[0031] Take the porous membrane PTFE (the film thickness is about 160 μm and the pore diameter is 5 μm), the FEP film (the film thickness is about 50 μm and the pore diameter is 5 μm), and melt at 300 ° C for 20 minutes to prepare the PTFE / FEP electret film. Needle voltage -12kv, electret at room temperature for 1min, preparation surface voltage is -1kv. Store in a desiccator for later use.
[0032] Take 30g of notoginseng fine powder, extract with 300ml of ethanol under reflux, and extract 3 times, each time for 1h. The extracts were combined and concentrated, evaporated to dryness under reduced pressure, weighed 1 g of the dried product, and dissolved it with 1 g of dragon's blood fine powder, and dissolved it in 200 ml of ethanol to prepare a liquid with a concentration of 10 mg / ml. Take a PP film (film thickness 13 μm, pore diameter 5 μm), soak it in the liquid medicine, take it out after 8 hours, and dry i...
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