Method of manufacturing nano-carbon packaged copper nano-particle and application of the same as heat conduction filling material
A technology of nano-particles and thermally conductive fillers, applied in coatings and other directions, can solve the problems of no related reports, low thermal expansion coefficient, poor corrosion resistance, etc., and achieve the effect of improving deformation ability, efficient heat dissipation function, and high effect
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Embodiment 1
[0009] Weigh the pure copper powder containing 10% copper and mix it with pure graphite powder to make an anode composite rod, and use a pure graphite rod for the cathode, put the two electrodes into the reaction chamber, adopt the DC carbon arc method, and feed high-purity Ar gas, The reaction voltage is 20V, the current is 60A, and the Ar pressure is 10kPa, and the deep black fluffy carbon-coated copper nanoparticles are reacted under arc discharge. The morphology and particle size of carbon-coated copper nanoparticles are observed by transmission electron microscope, and its outer diameter is 20-50nm. The use of carbon-coated copper nanoparticle fillers evenly dispersed in silicone oil can significantly improve the thermal conductivity of the system. When the filler weight When the percentage reaches 1%, the thermal conductivity of silicone oil can be increased by 40%.
Embodiment 2
[0011] Weigh the pure copper powder containing 30% copper and mix it with pure graphite powder to make an anode composite rod, and use a pure graphite rod for the cathode, put the two electrodes into the reaction chamber, adopt the DC carbon arc method, and feed high-purity Ar gas, The reaction voltage is 23V, the current is 120A, and the Ar pressure is 30kPa, and the deep black fluffy carbon-coated copper nanoparticles are reacted under arc discharge. The morphology and particle size of carbon-coated copper nanoparticles are observed by transmission electron microscope, and its outer diameter is 35-60nm. Using carbon-coated copper nanoparticle fillers evenly dispersed in silicone oil can significantly improve the thermal conductivity of the system. When the filler weight The percentage reaches 2%, and the thermal conductivity of silicone oil can be increased by 60%.
Embodiment 3
[0013] Weigh the pure copper powder containing 50% copper and mix it with pure graphite powder to make an anode composite rod, and use a pure graphite rod for the cathode, put the two electrodes into the reaction chamber, adopt the DC carbon arc method, and feed high-purity Ar gas, The reaction voltage is 25V, the current is 150A, and the Ar pressure is 50kPa. Under the arc discharge, dark black fluffy carbon-coated copper nanoparticles are obtained. The morphology and particle size of carbon-coated copper nanoparticles are observed by transmission electron microscope, and its outer diameter is 40-80nm. Using carbon-coated copper nanoparticles fillers evenly dispersed in silicone oil can significantly improve the thermal conductivity of the system. When the filler weight The percentage reaches 3%, and the thermal conductivity of silicone oil can be increased by 80%.
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