Initial magnetic-inductive capacity 100 (+20) (-20) nickel-zinc ferrite material and preparation method
A technology of nickel-zinc ferrite and initial magnetic permeability, applied in the direction of magnetism of inorganic materials, can solve the problems of ferrite eddy current loss increase, increase production cost, reduce lamp efficiency, etc., achieve good temperature characteristics, reduce usage Small, the effect of improving the electromagnetic loss characteristics
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Embodiment 1
[0032] 1) Selection of raw materials: This embodiment provides a nickel-zinc ferrite material with an initial permeability of 112 and a preparation method, and the raw material is industrially pure Fe 2 O 3 , ZnO, MnCO 3 , NiO and CoO.
[0033] 2) Composition design and weighing: according to Fe 2 O 3 49mol%, ZnO 16mol%, MnCO 3 It is 1 mol%, NiO is 33.7 mol%, and CoO is 0.3 mol%.
[0034] 3) Mixing of raw materials: Put the weighed raw materials into a sand mill, add deionized water, the weight of the deionized water is 1.2 times the total weight of the raw materials, and the ball milling time is 2 hours.
[0035] 4) Pre-burning: Dry the raw materials that have been ball-milled once, and put them into an electric furnace for pre-burning. The pre-burning temperature is 950°C, and the pre-burning time is 3.5 hours. After calcining, XRD phase analysis was performed on the calcined material, and it was determined that only the spinel structure existed in the calcined material, and the...
Embodiment 2
[0043] 1) Selection of raw materials: This embodiment provides a nickel-zinc ferrite material with an initial permeability of 102 and a preparation method, and the raw material is industrially pure Fe 2 O 3 , ZnO, MnCO 3 , NiO and CoO.
[0044] 2) Composition design and weighing: according to Fe 2 O 3 46mol%, ZnO 12.4mol%, MnCO 3 It is 0.1 mol%, NiO is 40 mol%, and CoO is 1.5 mol%.
[0045] 3) Mixing of raw materials: Put the weighed raw materials into a sand mill, add deionized water, the weight of the deionized water is 1.2 times the total weight of the raw materials, and the ball milling time is 1 hour.
[0046] 4) Pre-burning: Dry the raw materials that have been ball-milled once and put them into an electric furnace for pre-burning. The pre-burning temperature is 1100°C, and the pre-burning time is 1.5 hours. After pre-burning, it is cooled in the furnace. After calcining, XRD phase analysis was performed on the calcined material, and it was determined that only the spinel st...
Embodiment 3
[0054] 1) Selection of raw materials: This embodiment provides a nickel-zinc ferrite material with an initial permeability of 92 and a preparation method, and the raw material is industrially pure Fe 2 O 3 , ZnO, MnCO 3 , NiO and CoO.
[0055] 2) Composition design and weighing: according to Fe 2 O 3 Is 49mol%, ZnO is 10mol%, MnCO 3 It is 0.4 mol%, NiO is 40 mol%, and CoO is 0.6 mol%.
[0056] 3) Mixing of raw materials: Put the weighed raw materials into a sand mill, add deionized water, the weight of the deionized water is 1.2 times the total weight of the raw materials, and the ball milling time is 1.5 hours.
[0057] 4) Pre-burning: Dry the raw materials that have been ball-milled once and put them into an electric furnace for pre-burning. The pre-burning temperature is 1000°C, and the pre-burning time is 2 hours. After pre-burning, it is cooled in the furnace. After calcining, XRD phase analysis was performed on the calcined material, and it was determined that only the spine...
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