Initial magnetic-inductive capacity 60 (+12) (-12) nickel-zinc ferrite material and preparation method
A technology of nickel-zinc ferrite and initial magnetic permeability, applied in the direction of inorganic material magnetism, can solve the problems of ferrite eddy current loss increase, increase production cost, reduce lamp efficiency, etc., and achieve good product consistency and wide frequency The effect of low electromagnetic loss and good wide temperature stability
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Embodiment 1
[0032] 1) Selection of raw materials: a kind of nickel-zinc ferrite material with an initial magnetic permeability of 68 and its preparation method provided in this embodiment, its raw material is selected industrially pure Fe 2 o 3 , ZnO, MnCO 3 , NiO and CoO.
[0033] 2) Composition design and weighing: according to Fe 2 o 3 49mol%, ZnO 14mol%, MnCO 3 1 mol%, NiO 35.7 mol%, and CoO 0.3 mol%.
[0034] 3) Mixing of raw materials: Put the weighed raw materials into a sand mill, add deionized water, the weight of deionized water is 1.2 times of the total weight of raw materials, and the ball milling time is 2 hours.
[0035] 4) Pre-burning: Dry the raw materials that have been ball-milled once, and put them into an electric furnace for pre-burning. The pre-burning temperature is 950°C, and the pre-burning time is 3.5 hours. After pre-burning, it is cooled with the furnace. After pre-burning, XRD phase analysis was carried out on the pre-fired material, and it was confirmed...
Embodiment 2
[0043] 1) Selection of raw material: a kind of nickel-zinc ferrite material and preparation method with an initial magnetic permeability of 61 provided in this embodiment, its raw material selects industrially pure Fe 2 o 3 , ZnO, MnCO 3 , NiO and CoO.
[0044] 2) Composition design and weighing: according to Fe 2 o 3 46mol%, ZnO 10.4mol%, MnCO 3 0.1 mol%, NiO 42 mol%, and CoO 1.5 mol%.
[0045] 3) Mixing of raw materials: Put the weighed raw materials into a sand mill, add deionized water, the weight of deionized water is 1.2 times of the total weight of raw materials, and the ball milling time is 1 hour.
[0046] 4) Pre-burning: Dry the raw materials that have been ball-milled once, and put them into an electric furnace for pre-burning. The pre-burning temperature is 1100°C, and the pre-burning time is 1.5 hours. After pre-burning, it is cooled with the furnace. After pre-burning, XRD phase analysis was carried out on the pre-fired material, and it was confirmed that o...
Embodiment 3
[0054] 1) Selection of raw material: a kind of nickel-zinc ferrite material and preparation method with an initial magnetic permeability of 52 provided in this embodiment, its raw material selects industrially pure Fe 2 o 3 , ZnO, MnCO 3 , NiO and CoO.
[0055] 2) Composition design and weighing: according to Fe 2 o 3 49mol%, ZnO 8mol%, MnCO 3 0.4 mol%, NiO 42 mol%, and CoO 0.6 mol%.
[0056] 3) Mixing of raw materials: Put the weighed raw materials into a sand mill, add deionized water, the weight of deionized water is 1.2 times of the total weight of raw materials, and the ball milling time is 1.5 hours.
[0057] 4) Pre-burning: Dry the raw materials that have been ball-milled once, and put them into an electric furnace for pre-burning. The pre-burning temperature is 1000°C, and the pre-burning time is 2 hours. After pre-burning, it is cooled with the furnace. After pre-burning, XRD phase analysis was carried out on the pre-fired material, and it was confirmed that onl...
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