Initial magnetic-inductive capacity 40 (-8) (+8) nickel-zinc ferrite material and preparation method
A nickel-zinc ferrite and initial magnetic permeability technology, applied in the direction of inorganic material magnetism, can solve the problems of rising eddy current loss of ferrite, reducing lamp efficiency, increasing production cost, etc., to reduce electromagnetic loss and ensure normal stability The effect of working, broadband and low electromagnetic loss
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Embodiment 1
[0029] 1) Selection of raw materials: a kind of nickel-zinc ferrite material with an initial magnetic permeability of 46 and its preparation method provided in this embodiment, its raw material selects industrially pure Fe 2 o 3 , ZnO, MnCO 3 , NiO and CoO.
[0030] 2) Composition design and weighing: according to Fe 2 o 3 49mol%, ZnO 8mol%, MnCO 3 1mol%, NiO 41.7mol% and CoO 0.3mol%;
[0031] 3) Mixing of raw materials: put the weighed raw materials into a sand mill, add deionized water, the weight of deionized water is 1.2 times of the total weight of raw materials, and the ball milling time is 2 hours;
[0032] 4) Pre-burning: Dry the raw materials that have been ball-milled once, and put them into an electric furnace for pre-burning. The pre-burning temperature is 950°C, and the pre-burning time is 3.5 hours. After pre-burning, it is cooled with the furnace. After pre-burning, conduct XRD phase analysis on the pre-fired material to confirm that only spinel structure ...
Embodiment 2
[0042] 1) Selection of raw material: a kind of nickel-zinc ferrite material and preparation method with an initial magnetic permeability of 39 provided in this embodiment, its raw material selects industrially pure Fe 2 o 3 , ZnO, MnCO 3 , NiO and CoO.
[0043] 2) Composition design and weighing: according to Fe 2 o 3 46mol%, ZnO 4.4mol%, MnCO 3 0.1 mol%, NiO 48 mol%, and CoO 1.5 mol%.
[0044] 3) Mixing of raw materials: Put the weighed raw materials into a sand mill, add deionized water, the weight of deionized water is 1.2 times of the total weight of raw materials, and the ball milling time is 1 hour.
[0045] 4) Pre-burning: Dry the raw materials that have been ball-milled once, and put them into an electric furnace for pre-burning. The pre-burning temperature is 1100°C, and the pre-burning time is 1.5 hours. After pre-burning, it is cooled with the furnace. After pre-burning, XRD phase analysis was carried out on the pre-fired material, and it was confirmed that on...
Embodiment 3
[0055] 1) Selection of raw material: a kind of nickel-zinc ferrite material and preparation method with an initial magnetic permeability of 34 provided in this embodiment, its raw material selects industrially pure Fe 2 o 3 , ZnO, MnCO 3 , NiO and CoO.
[0056] 2) Composition design and weighing: according to Fe 2 o 3 49mol%, ZnO 2mol%, MnCO 3 0.4 mol%, NiO 48 mol%, and CoO 0.6 mol%.
[0057] 3) Mixing of raw materials: Put the weighed raw materials into a sand mill, add deionized water, the weight of deionized water is 1.2 times of the total weight of raw materials, and the ball milling time is 1.5 hours.
[0058] 4) Pre-burning: Dry the raw materials that have been ball-milled once, and put them into an electric furnace for pre-burning. The pre-burning temperature is 1000°C, and the pre-burning time is 2 hours. After pre-burning, it is cooled with the furnace. After pre-burning, XRD phase analysis was carried out on the pre-fired material, and it was confirmed that onl...
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