Supercritical carbonic anhydride wall-breaking method for melissa powder
A technology of carbon dioxide and bee pollen, applied in the fields of natural product health care products and pharmaceuticals, can solve the problems of long time required for wall breaking, increase product cost, and cannot be popularized and used, and achieves easy operation, energy saving, and beneficial nutrients. saved effect
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Embodiment 1
[0027] Vacuum-dry fresh bee pollen to a moisture content of 6.20%, take 300g of dried pollen and put it into a 1L extractor, and use carbon dioxide with a purity of 99% to boost the pressure of the extraction vessel to a pressure of 15MPa at the temperature of the extraction vessel at 35°C; After 5 minutes of pressure, open the exhaust valve of the extraction tank to quickly empty the carbon dioxide and collect the pollen. Electron microscopy showed that the pollen cells had been broken.
Embodiment 2
[0029] Weigh 300g of dried bee pollen and put it into a 1L extractor. Under the condition of the temperature of the extraction tank at 35°C, use carbon dioxide with a purity of 99% to boost the pressure of the extraction tank to 30 MPa; keep the pressure for 5 minutes and then open the exhaust valve of the extraction tank to quickly discharge Empty carbon dioxide and collect pollen. Electron microscopy showed that the pollen cells had been broken.
Embodiment 3
[0031] Vacuum-dry the fresh bee pollen until the water content is 6.20%, take 300g of the dried pollen and put it into the 11 extractor, and under the condition of the temperature of the extraction kettle at 40°C, use carbon dioxide with a purity of 99% to boost the pressure of the extraction kettle to 30MPa; After maintaining the pressure for 10 minutes, open the exhaust valve of the extraction tank to quickly empty the carbon dioxide; just take out the pollen. Electron microscopy showed that the pollen cells had been broken.
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