Special organosilicon adhesive for fire-resistant isinglass belt and production method
A technology of silicone adhesive and refractory mica, which is applied in the direction of mica, adhesives, inorganic insulators, etc., can solve the problems of back sticking, poor dryness, moisture absorption, etc., and achieve good adhesion, good cohesiveness, and softness Good results
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Embodiment 1
[0018] Take a 250ML three-necked flask, add 40 g of toluene, 12 g of MQ resin, and 50 g of silicone rubber, install a stirrer, a thermometer and a reflux condenser, turn on the stirrer, add 0.006 g of sodium acetate, and heat to reflux for 6 hours at a temperature of 112°C. Add 1 drop (0.05g) of lower alcohol polymerization inhibitor, stir for 20 minutes, and cool for use after uniformity. When used, add 0.48g of dibenzoyl peroxide, stir evenly, coat it on the mica tape and bake it at 80℃ for 3 minutes, and cure it at 150℃ for 3 minutes.
Embodiment 2
[0020] Take a 250ML three-necked flask, add 30 g of toluene, 20 g of MQ resin, and 40 g of silicone rubber. Install the stirring, thermometer and reflux condenser, turn on the stirring, add 0.010 g of sodium acetate, and heat to reflux for 6 hours at a temperature of 112°C. Add 2 drops (0.1 g) of polymerization inhibitor, stir for 20 minutes, and cool for use after uniformity. When used, add 0.48g of dibenzoyl peroxide, stir evenly, coat it on the mica tape and bake it at 80℃ for 3 minutes, and cure it at 150℃ for 3 minutes.
Embodiment 3
[0022] Take a 250ML three-necked flask, add 25 g of toluene, 22 g of MQ resin, and 38 g of silicone rubber, install a stirrer, a thermometer and a reflux condenser, turn on the stirring, add 0.015 g of sodium acetate, and heat to reflux for 6 hours at a temperature of 112°C. Add 2 drops (0.1 g) of polymerization inhibitor, stir for 20 minutes, and cool for use after uniformity. When used, add 0.48g of dibenzoyl peroxide, stir evenly, coat it on the mica tape and bake it at 80℃ for 3 minutes, and cure it at 150℃ for 3 minutes.
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