Silicon rubber chemical copper-plating technique
A technology of electroless copper plating and silicone rubber, which is applied in the direction of liquid chemical plating, metal material coating technology, coating, etc., can solve the problems of copper plating on silicone rubber substrates, etc., and achieve good flexibility, stable work, cost saving effect
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Embodiment 1
[0013] Embodiment 1: Embodiment 1: select silicon rubber for use, put it into sodium hydroxide (NaOH) of 10 / L, sodium carbonate (Na2CO3) of 35g / L and trisodium phosphate (Na3PO3 12H2O) of 25g / L In the three-alkali solution composed, soak at a constant temperature of 80°C for 30 minutes to remove oil, and then wash with deionized water after degreasing; roughen with 200ml / L hydrochloric acid solution (HCl) solution for 2min, and then wash with deionized water; wash with 10g / L stannous chloride (SnCl2 6H2O) and 40ml / L hydrochloric acid solution (HCl) prepared solution sensitization 3min, then wash with deionized water; use 5g / L silver nitrate (AgNO3) and 10ml / L of ammonia water (NH3·H2O) was activated for 4 minutes and washed with deionized water; finally put it into the plating solution for electroless plating, the temperature was 22°C, the pH value was 12.5, and copper plating could be done after 30 minutes get the product. The plating solution consists of 18g / L copper sulf...
Embodiment 2
[0014] Example 2: Silicone rubber is soaked in 15 / L of sodium hydroxide (NaOH), 25g / L of sodium carbonate (Na2CO3) and 35g / L of trisodium phosphate (Na3PO3 12H2O) at a constant temperature of 80°C for 35min before use. Rinse with deionized water; roughen with 150ml / L hydrochloric acid solution (HCl) for 2 minutes and wash with deionized water; prepare with 12g / L stannous chloride (SnCl2 6H2O) and 40ml / L hydrochloric acid solution (HCl) Wash the resulting solution with deionized water after sensitization for 3 minutes; wash with deionized water after activating the solution prepared with 4g / L silver nitrate (AgNO3) and 10ml / L ammonia water (NH3·H2O) for 5min; finally Electroless copper plating is carried out at a temperature of 25°C and a pH of 12.5, and the product will be ready in 30 minutes. The plating solution consists of 15g / L copper sulfate (CuSO4 5H2O), 12ml / L formaldehyde (HCHO), 12g / L disodium ethylenediaminetetraacetic acid (EDTA (C10H14N2Na2O8 12H2O)), 15mg / L ferrou...
Embodiment 3
[0015] Example 3: Silicone rubber is soaked in 20 / L sodium hydroxide (NaOH), 20g / L sodium carbonate (Na2CO3) and 50g / L trisodium phosphate (Na3PO3·12H2O) solution at a constant temperature of 80°C for 40min before use. Rinse with deionized water; roughen with 250ml / L hydrochloric acid solution (HCl) for 3 minutes and wash with deionized water; prepare with 15g / L stannous chloride (SnCl2 6H2O) and 40ml / L hydrochloric acid solution (HCl) The solution was sensitized for 4 minutes and washed with deionized water; the solution prepared with 4g / L silver nitrate (AgNO3) and 10ml / L ammonia water (NH3·H2O) was activated for 4 minutes and then washed with deionized water; finally, the chemical Copper plating, the temperature is 25°C, the pH value is 13, and the product can be obtained after 25 minutes. The plating solution consists of 20g / L copper sulfate (CuSO4 5H2O), 14ml / L formaldehyde (HCHO), 16g / L disodium ethylenediaminetetraacetic acid (EDTA (C10H14N2Na2O8 12H2O)), 20mg / L ferrous...
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