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Method of producing adenosine disodium triphosphate

A technology of adenosine triphosphate disodium and its production method, which is applied in sugar derivatives, organic chemistry, etc., can solve the problems of high production cost, heavy environmental pollution, complicated operation, etc., and achieve the effects of ensuring health, reducing environmental pollution, and reducing pollution

Inactive Publication Date: 2007-08-08
张剑
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Adenosine triphosphate disodium (ATP-Na 2 ) production method, the operation is complex, the production cost is high, the use of solvent toluene, the discarded yeast cannot be fully utilized, the environmental pollution is large, and the product conversion rate is low and the yield is low

Method used

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Examples

Experimental program
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Effect test

Embodiment Construction

[0030] A production method of adenosine triphosphate disodium, comprising the following steps:

[0031] (1) First add tap water to the reaction pot, start stirring at the same time, heat it to 43-45°C with a jacket, then add sucrose, glucose, potassium dihydrogen phosphate, and dipotassium hydrogen phosphate to dissolve them, stop heating, and use a circulation The water cools down. When the temperature drops below 40-42°C, put in yeast mud and heat up slowly with a jacket.

[0032] (2) Dissolve magnesium sulfate with tap water twice the volume of magnesium sulfate, and in addition, heat tap water to 80° C. to dissolve adenosine at a ratio of water: adenosine solution = 12:1.

[0033] (3) When the temperature in the reaction pot reaches 25°C±1°C, add magnesium sulfate and adenosine solution in sequence. And heat the reaction feed liquid to 38-40°C, stop heating, and keep it warm for 2 hours. At this time, start sampling to measure the conversion rate of adenosine. If there ar...

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Abstract

The invention discloses a manufacturing method of tribiofosfor, which comprises the following steps: reacting; inactivating; separating through resin; decoloring; hyperfiltering; crystallizing.

Description

Technical field: [0001] The invention relates to a production method of adenosine triphosphate disodium. Background technique: [0002] Adenosine triphosphate disodium (ATP-Na 2 ) production method, complex operation, high production cost, use of solvent toluene, discarded yeast can not be fully utilized, environmental pollution is large, and the product conversion rate is low and the yield is low. Invention content: [0003] The object of the present invention is to provide a kind of production method of adenosine triphosphate disodium with high product conversion rate and high ATP yield. [0004] Technical solution of the present invention is: [0005] A kind of production method of adenosine triphosphate disodium, it is characterized in that: comprise the following steps: [0006] (1) First add tap water to the reaction pot, start stirring at the same time, heat it to 43-45°C with a jacket, then add sucrose, glucose, potassium dihydrogen phosphate, and dipotassium hy...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07H19/20
Inventor 张剑
Owner 张剑
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