Process of extracting mannitol using glucose mother liquid
A technology of glucose mother liquor and mannitol, which is applied in the directions of blood diseases, extracellular fluid diseases, fermentation, etc., can solve the problems of unretrieved mannitol method, immature high-purity fructose technology, and incompatibility with industrialized large-scale production, etc. The effect of production cost, increasing added value and improving utilization rate
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Embodiment 1
[0040] (1) 5L of glucose mother liquor A (dry matter 52.4%, from Shanxi Xiwang Sugar Industry Co., Ltd.), diluted with deionized water to a dry matter weight percentage concentration of 30%, is then filtered through a nanofiltration membrane device to obtain a concentration of 20.5% respectively The glucose-rich component B and the concentration of 32.75% oligosaccharide-rich component C;
[0041] (2) Adjust the pH of oligosaccharide-rich component C to 4.3 with hydrochloric acid, saccharify at 58°C for 55 hours, then combine with glucose mother liquor A, repeat mother liquor A nanofiltration→saccharification of C liquor→saccharify with glucose mother liquor A Merge→the steps of (1) and (2) of mother liquor A nanofiltration again;
[0042] (3) The glucose-rich component B obtained in the step (1) is deionized through cation exchange resin AmberliteIRC76CRF+Amberlite FPRC22Na, anion exchange resin Amberlite FPA51+Amberlite FPA90C1; then vacuum concentration to dry matter weight...
Embodiment 2
[0049] (1) Dilute 5L of glucose mother liquor A (dry matter 60%) with deionized water to a dry matter weight percentage concentration of 35%, then filter the nanofiltration membrane device to obtain the glucose-rich component B and the oligosaccharide-rich group respectively share C;
[0050] (2) Adjust the pH of oligosaccharide-rich component C to 4.5 with hydrochloric acid, saccharify at 60°C for 45 hours, then combine with glucose mother liquor A, and then repeat nanofiltration of mother liquor A → saccharification of liquid C → saccharification with glucose mother liquor A Merge→the steps of (1) and (2) of mother liquor A nanofiltration again;
[0051] (3) The glucose-rich component B obtained in the step (1) is deionized through cation exchange resin AmberliteIRC76CRF+Amberlite FPRC22Na, anion exchange resin Amberlite FPA51+Amberlite FPA90C1; then vacuum concentration to dry matter weight percent concentration is 60%; Add 1.5% molybdate catalyst by relative dry matter we...
Embodiment 3
[0057] (1) Dilute 5L glucose mother liquor A (dry matter 50%) with deionized water to a dry matter weight percent concentration of 25%, and then filter a nanofiltration membrane device to obtain respectively a glucose-rich component B and an oligosaccharide-rich group share C;
[0058] (2) Adjust the pH of oligosaccharide-rich component C to 4.2 with hydrochloric acid, saccharify at 55°C for 55 hours, then combine with glucose mother liquor A, and then repeat nanofiltration of mother liquor A → saccharification of liquid C → saccharification with glucose mother liquor A Merge→the steps of (1) and (2) of mother liquor A nanofiltration again;
[0059] (3) The glucose-rich component B obtained in the step (1) is deionized through cation exchange resin AmberliteIRC76CRF+Amberlite FPRC22Na, anion exchange resin Amberlite FPA51+Amberlite FPA90Cl; then vacuum concentration to dry matter weight percent concentration is 40%; Add 2% molybdate catalyst by relative dry matter weight to t...
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