Production method of diesel oil by supersonic methanol esterification
A biodiesel and ultrasonic technology, applied in the preparation of biological raw materials, liquid hydrocarbon mixtures, petroleum industry, etc., can solve the problems of difficult recovery, short service life of enzymes, waste lye discharge, etc., to simplify the production process and production costs, Improve the conversion rate and avoid the effect of pollution
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Embodiment 1
[0022] In a conventional reaction vessel welded by a stainless steel plate equipped with an ultrasonic vibrator, methanol and waste oil are mixed in a molar ratio of 30:1, the temperature is controlled at 60°C, and the motor drives the stirrer to stir at a speed of 1500r / min. Promote the uniform mixing of methanol and raw oil; turn on the power of the ultrasonic generator, adjust the ultrasonic frequency generated by the ultrasonic vibrator to 30kHz, and the power to be 2kw. The ultrasonic waves emitted by the ultrasonic vibrator will produce cavitation, heating and high-frequency oscillation in the reactant It can increase the activity of the reactants, promote the formation of free radicals in the reactants and the occurrence of cracking reactions, and make the molecules of the reactants collide strongly with each other, so as to accelerate the complete chemical reaction of methanol esterification to produce biodiesel. , after carrying out the transesterification reaction for...
Embodiment 2
[0024] In the reaction vessel described in Example 1, methanol and animal waste fat were mixed in a molar ratio of 20:1, at 40°C, with a stirring speed of 1800r / min, ultrasonic power of 5kw and ultrasonic frequency of 20kHz, for 1.5 hour transesterification reaction. The reacted mixed solution was left to stand for 12 hours, the mixed solution was separated into layers, and the glycerol in the lower layer was separated; the upper mixed solution was distilled at 100° C. until all the methanol was recovered, and the remaining distillate was biodiesel.
Embodiment 3
[0026] In the reaction vessel described in Example 1, methanol and waste cooking oil from the catering industry are mixed in a molar ratio of 50:1, at 64°C, stirring speed 2000r / nin, ultrasonic power is 10kw and ultrasonic frequency 60kHz. 1 hour transesterification reaction. The reacted mixed solution was left to stand for 10 hours, the mixed solution was layered, and the glycerin in the lower layer was separated; the upper mixed solution was distilled at 80° C. until all the methanol was recovered, and the remaining distillate was biodiesel.
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