Filling and insulating mould coating of titanium dioxide coating fly ash float and preparation method thereof
A technology of fly ash floating beads and titanium dioxide, which is applied in chemical instruments and methods, fireproof coatings, fibrous fillers, etc., can solve the problems of thick insulation layer, poor convection and radiation heat transfer effect, and inability to block heat transfer, etc. The effect of improving utilization and thermal reflectivity
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Embodiment 1
[0049] Example 1 Preparation of titanium dioxide-coated fly ash floating beads filler
[0050] Mix 50g of distilled water with a particle size of 70-80um and a specific surface area of 0.4-0.5m 2 The fly ash floating pearl 5g of / g adds in the four-necked flask, and the concentration that drips 0.3ml in this four-necked flask is the surfactant sodium dodecylbenzene sulfonate aqueous solution of 0.1g / ml, fully stirs, Make the fly ash floating bead suspension; under the electric stirrer with 60 rev / min constant speed stirring state, dropwise the mass percentage concentration of 286.7g in this fly ash floating bead suspension in the reaction time of 6 hours is 10% Titanium sulfate aqueous solution, and maintain the pH value at 2.0 to 2.5 by dropwise adding 0.1g / ml sodium hydroxide solution to maintain the reaction time, let it stand for 2 hours, filter, wash until the filtrate is added with sodium hydroxide Until there is no white precipitate, the powder is obtained by suction...
Embodiment 2
[0051] Example 2 Prepare the filler of titanium dioxide coated fly ash floating beads
[0052] Mix 60g of distilled water with a particle size of 70-80um and a specific surface area of 0.4-0.5m 2 The fly ash floating pearl 5g of / g adds in the four-necked flask, and in this four-necked flask, drips the surfactant sodium dodecylbenzene sulfonate aqueous solution of the concentration 0.1g / ml of 0.2ml, fully stirs, prepares Fly ash floating bead suspension; under the state of stirring at a constant speed of 60 rpm with an electric stirrer, in the reaction time of 4 hours, dropwise add 126.1g of 126.1g mass percentage concentration to the fly ash floating bead suspension to be 15% titanyl sulfate aqueous solution, and keep the pH value at 2.0 to 2.5 by dropping 0.1g / ml potassium hydroxide solution to maintain the reaction time, let it stand for 2 hours, filter, wash until the filtrate is added with sodium hydroxide Until there is no white precipitate, the powder is obtained by ...
Embodiment 3
[0053] Example 3 Preparation of fillers coated with titanium dioxide fly ash floating beads
[0054] Mix 55g of distilled water with a particle size of 70-80um and a specific surface area of 0.4-0.5m 2 The fly ash floating pearl 5g of / g adds in the four-necked flask, and in this four-necked flask, drips the surfactant sodium dodecylbenzene sulfonate aqueous solution of the concentration 0.1g / ml of 0.2ml, fully stirs, prepares Fly ash floating bead suspension; under the electric agitator with 60 rev / min constant speed stirring state, in 8 hours reaction time in this fly ash floating bead suspension, the mass percent concentration of 140.2g is 20% Titanium sulfate aqueous solution, and maintain the pH value under the condition of 2.0~2.5 by dropping 0.1g / ml potassium hydroxide solution, keep the reaction time, let it stand for 2 hours, filter, wash until no sodium hydroxide is added in the filtrate Until the white precipitate was obtained, the powder was obtained by suction ...
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