Method for extracting series effective ingredient of pyracantha
A technology of active ingredients and extraction methods, which is applied in the field of extraction of active ingredients of Pyracantha series, can solve the problems of no comprehensive utilization research, single active ingredient, low resource utilization rate, etc., and achieve product safety, non-toxicity, low cost, The effect of high resource utilization
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[0033] Figure 1 shows the process flow of the present invention.
[0034] Non-limiting examples of the invention:
[0035] (1) Take 100 kg of fresh Pyracantha japonicus fruit after removing impurities and cleaning, add 100 kg of water, squeeze and filter with a juicer, and obtain 128-131 kg of Pyracantha japonicus juice, which is used as a fruit juice drink after deastringent and sterilized or fruit wine, etc.; the pomace is used for the next step of extraction.
[0036] (2) In the pomace after squeezing the juice, add 500 kg of 65% ethanol aqueous solution with a pH of 3, heat extraction at 30-45°C for 40-50 minutes or ultrasonic extraction for 20-25 minutes or microwave extraction for 3 ~ 6 minutes, or cold soak for 18 ~ 22 hours, filter out the solution, and extract the filter residue twice in the same way. Combine the extracts obtained three times, recover ethanol under reduced pressure, purify with macroporous resin or silica gel column chromatography, spray dry or free...
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