Composite cellulose viscose filament yarn with composite cellulose pulp as raw materials made of cotton, wood, hemp and bamboo mixture, and preparation method thereof
A technology of composite cellulose and viscose filaments, which is applied in the direction of cellulose/protein conjugated artificial filaments, spinning solution preparation, etc., can solve the problems of high cost and low production efficiency, and achieve low cost and optimized production process , glossy effect
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Embodiment 1
[0039] Production of 120D / 30F composite cellulose viscose filament:
[0040] Raw materials: Mix natural cotton, wood, hemp, bamboo, and carapace raw materials to make composite cellulose new pulp, wherein: the ratio of cotton, wood, hemp, bamboo, and carapace raw materials is: 30%: 20%: 20%: 20%: 10%
[0041] Dipping process:
[0042] Alkaline temperature: 35°C
[0043] Alkaline concentration: 188g / l
[0044] Dipping time: 100 minutes
[0045] Alkali fiber composition: α-cell content: 28%
[0046] NaOH content: 16.3%
[0047] Amount of VIF-64 added: 0.5% (for α-cell)
[0048] Amount of VIF-9 added: 1.0% (for α-cell)
[0049] Yellowing process:
[0050] CS 2 Added amount: 35.5% (for α-cell)
[0051] Yellowing temperature: 30°C
[0052] Yellowing time: 70 minutes
[0053] Dissolving temperature: 8°C
[0054] Amount of VIF-51 / 41 added: 2.0% (for α-cell)
[0055] Viscose before spinning:
[0056] α-cell content: 7.85%
[0057] NaOH content: 6.15%
[0058]...
Embodiment 2
[0084] Production of 600D / 100F composite cellulose viscose filament:
[0085] Raw materials: Mix natural cotton, wood and bamboo raw materials to make composite cellulose pulp, among which: the ratio of cotton, wood and bamboo raw materials is: 50%: 35%: 15%
[0086] Dipping process:
[0087] Alkaline temperature: 48°C
[0088] Alkaline concentration: 180g / l
[0089] Dipping time: 80 minutes
[0090] Alkali fiber composition: α-cell content: 32.3%
[0091] NaOH content: 15.8%
[0092] Amount of VIF-64 added: 1.0% (for α-cell)
[0093] The amount of VIF-9 added: 1.3% (for α-cell)
[0094] Yellowing process:
[0095] CS 2 Added amount: 30.5% (for α-cell)
[0096] Yellowing temperature: 26.5°C
[0097] Yellowing time: 80 minutes
[0098] Dissolving temperature: 13°C
[0099] Addition amount of VIF-51 / 41: 1.5% (for α-cell)
[0100] Viscose before spinning:
[0101] α-cell content: 8.03%
[0102] NaOH content: 5.98%
[0103] Viscosity (falling ball method):...
Embodiment 3
[0129] Production of 120D / 30F dull composite cellulose viscose filament:
[0130] Raw materials: Mix natural cotton, hemp and bamboo raw materials to make composite cellulose pulp, among which: the ratio of cotton, hemp and bamboo raw materials is: 60%: 15%: 25%
[0131] Dipping process:
[0132] Alkaline temperature: 42°C
[0133] Alkaline concentration: 216g / l
[0134] Dipping time: 90 minutes
[0135] Alkali fiber composition: α-cell content: 29.6%
[0136] NaOH content: 16.3%
[0137] Amount of VIF-64 added: 1.2% (for α-cell)
[0138] Amount of VIF-9 added: 1.0% (for α-cell)
[0139] Yellowing process:
[0140] CS 2 Added amount: 28.5% (for α-cell)
[0141] Yellowing temperature: 31°C
[0142] Yellowing time: 45 minutes
[0143] Dissolving temperature: 15°C
[0144] Addition amount of VIF-51 / 41: 1.5% (for α-cell)
[0145] Viscose before spinning:
[0146] α-cell content: 7.85%
[0147] NaOH content: 5.96%
[0148] Viscosity (falling ball method): 4...
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