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Process for preparing flaky heavy calcium carbonate

A heavy calcium carbonate, flake technology, applied in the direction of calcium carbonate/strontium/barium, dyeing physical treatment, etc., can solve problems such as environmental pollution, and achieve the effect of low cost

Inactive Publication Date: 2002-07-24
CHINA UNIV OF GEOSCIENCES (WUHAN)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The flaky calcium carbonate powder produced at present is flaky light calcium carbonate, and the easiest method is one-step method such as Japanese patent flat 2-184519 and Chinese patent CN1080909A, but the former uses a toxic crystal form control agent organic phosphine , the latter uses a low-toxic boride as a crystal form control agent, which is easy to pollute the environment
There is no report on the preparation of flaky heavy calcium carbonate by mechanical method

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0007] The preparation method of the flaky heavy calcium carbonate provided by the invention is: select structural alteration type calcite, and manufacture according to the following steps:

[0008] The raw materials are crushed by a crusher and then coarsely ground to 400 mesh with a Raymond mill.

[0009] The coarsely ground raw material is prepared into a slurry with a concentration of 65 wt%.

[0010] The flaker is used as wet ultra-fine grinding, with zirconia balls as the grinding medium, and it is divided into 7 stages of grinding, from the first level to the seventh level, the quality of the grinding medium φ0.8mm-1.2mm ball and φ1.5mm-2mm ball The ratios are 1:3, 1:2.5, 1:2, 1:1.5, 1:1, 1.5:1, 2:1 in turn. After grinding for 45 minutes, flaky ground calcium carbonate with a particle size of less than 2 microns and a content of 94% was obtained, and the diameter-thickness ratio of the sheet was greater than 5:1.

[0011] The invention is prepared by a mechanical meth...

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PUM

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Abstract

A process for preparing flaky heavy calcium carbonate includes choosing altered calcite or coarse-grain marble, pulverizing, preparing slurry, superfine ball grinding with zirconium (or aluminium) oxide balls with diameter of 0.5-1.2 mm and 1.5-2 mm in a ratio of (1-2):(1-3) for 30-60 min, pressing filtering and drying. Its advantages are low cost, no toxicity and no environmental pollution.

Description

technical field [0001] The invention relates to a preparation method of calcium carbonate powder, in particular to a preparation method of flaky ground calcium carbonate. Background technique [0002] Calcium carbonate powder can be used as a filler in papermaking, plastics, rubber, coatings, and adhesives to enhance mechanical and physical properties. The flaky calcium carbonate powder can improve the surface gloss and flatness of the product, especially in the paper industry, it can replace the flaky washed kaolin and be used as a top coating for copper plates and white papers. Calcium carbonate powder can be divided into two categories according to different preparation methods, one is prepared by chemical methods, called light calcium carbonate; the other is prepared by mechanical grinding method, called heavy calcium carbonate, Such as patent CN1161996A, its technological process is: 1, dry crushing and grinding of raw materials, 2, slurry mixing and dispersion, 3, wet...

Claims

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Application Information

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IPC IPC(8): C01F11/18C09C3/04
Inventor 张德沈上越李珍潘铁虹周明
Owner CHINA UNIV OF GEOSCIENCES (WUHAN)
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