Method for preparing spiral carbon nano pipe
A technology of carbon nanotubes and helical shapes, applied in the field of preparation of helical carbon nanotubes, can solve problems such as unsatisfactory research and application fields, and achieve the effects of low cost, simple processing technology and excellent performance
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[0015] After the manganese nodule minerals from the seabed are roughly crushed, they are ultrasonically cleaned in a large amount of clean water to remove dirt such as clay attached to the surface. Then ball mill and sieve the powder below 200 mesh to be used as catalyst.
[0016] Put the above-mentioned mineral catalyst into a quartz boat of a chemical vapor deposition device, heat to 750° C., and keep it warm for 20 minutes under a nitrogen atmosphere. Then feed acetylene gas at 80ml / min, catalyze the cracking reaction for 15 minutes, and obtain a product containing a large number of helical carbon nanotubes, the scanning electron microscope photo of which is shown in figure 1 .
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