Glossy ganoderma spore oil and its preparing method and use
A technology of Ganoderma lucidum spore oil and Ganoderma lucidum spore powder, which is applied in food preparation, application, pharmaceutical formulation, etc., can solve the problems of accelerating the oxidation and rancidity of oily substances, and affecting the quality of spore oil products.
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Embodiment 1
[0053] Embodiment 1 Get 5Kg of Ganoderma lucidum spore powder with broken walls, use 20% ethanol solution as wetting agent, make soft material, after extruding granulation, dry 5 hours at 45 ℃, get the spore powder granule that water content is 3.6% . Placed in a 50-liter supercritical carbon dioxide extraction kettle, CO 2 Pressurized by a high-pressure pump and circulated for extraction. The pressure of the extraction tank is 25MPa, the temperature is 40°C, the primary separation is 10MPa, 50°C, and the secondary separation is 5MPa, 40°C. After continuous extraction for 2.5 hours, the spore oil was collected in a separator to obtain light yellow spore oil with a special smell of spore powder. After centrifugation at 5000rpm, 1.082kg of oil was obtained, with a yield of 21.64%.
Embodiment 2
[0054] Embodiment 2 Get the ganoderma lucidum spore powder 5kg of broken wall, make wetting agent with 40% ethanol solution, make soft material, extrude granulation, dry 4 hours at 50 ℃, obtain the spore powder granule that water content is 4.3%. Placed in a 50-liter supercritical carbon dioxide extraction kettle, CO 2 CO pressurized by high pressure pump 2 Pressurized by a high-pressure pump and circulated for extraction. The pressure of the extraction kettle is 28MPa, the temperature is 45°C, the primary separation is 10MPa, 50°C, and the secondary separation is 6MPa, 40°C. After continuous extraction for 2 hours, the spore oil was collected in a separator to obtain light yellow spore oil with a special smell of spore powder. After centrifugation at 5000rpm, 1.189kg of oil was obtained, with a yield of 23.78%.
Embodiment 3
[0055] Embodiment 3. get the ganoderma lucidum spore powder 5kg of broken wall, make wetting agent with 10% ethanol solution, make soft material, extrude granulation, dry 6 hours at 35 ℃, get the spore powder granule that water content is 4.6% . Placed in a 50-liter supercritical carbon dioxide extraction kettle, CO 2 Pressurized by a high-pressure pump and circulated for extraction. The pressure of the extraction tank is 25MPa, the temperature is 45°C, the primary separation is 10MPa, 50°C, and the secondary separation is 6MPa, 40°C. After continuous extraction for 3 hours, the spore oil was collected in a separator to obtain light yellow spore oil with a special smell of spore powder. 1.142 kg of oil was obtained by centrifugation at 10000 rpm, with a yield of 22.84%.
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