Method for detecting heavy metal elements in polluted flow of soil-water interface of non-ferrous metal mining area

A non-ferrous metal and detection method technology, applied in the field of heavy metal detection, can solve the problems of non-movability, insufficient stability of atomic absorption spectrometer, automatic movement of atomic absorption spectrometer, etc., achieve low detection limit, significant application value and social benefits, and reduce The effect of pressure

Pending Publication Date: 2022-07-15
甘肃省有色金属地质勘查局兰州矿产勘查院
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Problems solved by technology

With the massive use of non-ferrous metals (such as antimony, lead, zinc, etc.) The heavy metal pollution flow at the water interface has caused the problem of complex heavy metal pollution in the water environment of non-ferrous metal mining areas and its surrounding areas and has become increasingly prominent. Atomic absorption spectroscopy can quickly measure the concentration of metal ions in the solution. When the atomic absorption spectrometer is in use, it is generally immovable. It increases the difficulty of moving. If it is designed to be movable, the atomic absorption spectrometer is prone to automatic movement when there is no staff to control it or when it is hit by a collision. The atomic absorption spectrometer is not stable enough, so we make improvements to this , a method for the detection of heavy metal elements in soil-water interface pollution flow in non-ferrous metal mining areas was proposed

Method used

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  • Method for detecting heavy metal elements in polluted flow of soil-water interface of non-ferrous metal mining area
  • Method for detecting heavy metal elements in polluted flow of soil-water interface of non-ferrous metal mining area
  • Method for detecting heavy metal elements in polluted flow of soil-water interface of non-ferrous metal mining area

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Embodiment

[0027] Example: as Figure 1-3 As shown, a method for detecting heavy metal elements in soil-water interface pollution flow in a non-ferrous metal mining area of ​​the present invention includes the following steps:

[0028] S1: Sample collection, use the collection tube to collect the samples in the pollution flow of the soil-water interface in the non-ferrous metal mining area, and use the random sampling method to sample different positions in the pollution flow;

[0029] S2: Sample processing, vacuum drying the collected samples, crushing and sieving after drying to obtain sample powder, and then adding the sample powder into a polytetrafluoroethylene pressure digestion tank, and digesting by adding a digestion solution to the tank. processing to obtain the solution to be tested;

[0030] S3: Prepare standard solution, prepare standard solution of heavy metals, measure the spectral intensity of the standard solution, draw the standard curve of the corresponding heavy meta...

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Abstract

The invention discloses a method for detecting heavy metal elements in a non-ferrous metal mining area soil-water interface pollution flow, which comprises the following steps: S1, sample collection: collecting samples in the non-ferrous metal mining area soil-water interface pollution flow by using a collection cylinder, and sampling different positions in the pollution flow by adopting a random sampling mode; s2, sample treatment: respectively carrying out vacuum drying on the collected samples, crushing and sieving after drying to obtain sample powder, adding the sample powder into a polytetrafluoroethylene pressure digestion tank, and adding a digestion solution into the tank for digestion treatment to obtain a solution to be detected. According to the method for detecting the heavy metal elements in the soil-water interface pollution flow of the non-ferrous metal mining area, the atomic absorption spectrometer is adopted for detection, the detection limit is low, the detection sensitivity and accuracy are high, operation is easy and convenient, the pollution degree is rapidly detected, assistance is provided for follow-up treatment and maintenance, and great application value and social benefits are achieved.

Description

technical field [0001] The invention relates to the technical field of heavy metal detection, in particular to a method for detecting heavy metal elements in soil-water interface pollution flow in non-ferrous metal mining areas. Background technique [0002] The soil-water interface pollution flow is a composite pollution fluid produced by the polluted soil under the action of rainfall or snowmelt runoff. The pollutants include various heavy metals, persistent organic matter and nutrients such as nitrogen and phosphorus, and are also non-point source pollution. a special form of expression. [0003] Non-ferrous metals (such as Sb, As, Pb, Cd, Cr, Cu, Zn, Hg, etc.) are global environmental pollutants, all of which are chronically toxic and carcinogenic to humans and organisms. With the large-scale use of non-ferrous metals (such as antimony, lead, zinc, etc.) in various industries and large-scale mining and beneficiation, a large number of associated heavy metals enter the s...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/01G01N21/31F16M11/04F16M11/18F16M11/24F16M11/42
CPCG01N21/01G01N21/3103F16M11/04F16M11/18F16M11/24F16M11/42
Inventor 贾艳黄登丽
Owner 甘肃省有色金属地质勘查局兰州矿产勘查院
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