Slag agent for external refining iron and titanium removal of industrial silicon furnace

A technology of silicon furnace and iron removal, which is applied in the direction of silicon compounds, chemical instruments and methods, inorganic chemistry, etc., can solve the problems of low content and difficult removal, so as to reduce activity, increase metal yield, and improve purity Effect

Pending Publication Date: 2022-04-15
GUIZHOU INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the reducibility of titanium is not much different from that of silicon, and the content is relatively small, so it is currently difficult to remove it by traditional oxygen blowing methods.
At the same time, since silicon is more reductive than iron, it is difficult to remove it by oxidation

Method used

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  • Slag agent for external refining iron and titanium removal of industrial silicon furnace
  • Slag agent for external refining iron and titanium removal of industrial silicon furnace
  • Slag agent for external refining iron and titanium removal of industrial silicon furnace

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Embodiment Construction

[0016] The invention provides a silicon-coated refining slag suitable for reducing the content of iron and titanium in industrial silicon. The technical problem solved by the slag agent in the invention is to remove And reduce impurity elements iron and titanium in industrial silicon. It is conducive to improving the purity and grade of industrial silicon, reducing the loss of elemental silicon in the process of blowing refining, shortening the refining time, and improving refining efficiency

[0017] Specifically, the present invention achieves the above-mentioned purpose by adding and adjusting the chemical ratio of the slag agent, and its chemical composition weight percentage meets: 5%2 2 2 O, Na 2 O, MgF 2 One or two or three of the three components form a combination, 5%2 O2 O2 2 o 3 +M No<1%; the rest are impurities.

[0018] The CEO / SiO 2 0.1 to 0.6.

[0019] The carbon (C) in the composition is provided by one, two or three of graphite, carbon black and coal powd...

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Abstract

The invention relates to a slag agent for external refining iron and titanium removal of industrial silicon, which is used for achieving the purpose of refining iron and titanium removal. The invention relates to a slag agent for removing iron and titanium in external refining of industrial silicon. The slag agent comprises the following characteristic components (in percentage by mass): 5% lt; cEOlt, CEOlt; 15%; 4% lt; caF2 < 1t >; 15%; 40% lt; siO2 < 1t >; one or two or three of Li2O, Na2O and MgF2 form a combined body, and 5% 1t of Li2O, Na2O and MgF2; the combination is lt; 25%, and satisfies Li2Olt; 10% of Na2O1t, 10% of Na2O1t; 17%, MgF2 < 1t >; 8%; 2% lt; clt; 18%; bOlt; 5%; and Fe2O3 + MNot, Fe2O3 + MNot; 1%; the balance is impurities. The slag agent disclosed by the invention is used for external refining of industrial silicon and is matched with blowing refining of a silicon ladle, so that the content of iron and titanium brought into the industrial silicon by crude fuel can be remarkably reduced on the basis of not influencing refining and dealumination, and the stability of a refining process is not influenced.

Description

technical field [0001] The invention relates to the technical field of out-of-furnace refining in industrial silicon production, in particular to a slag agent used for removing iron and titanium in out-of-furnace refining of industrial silicon, which can remove aluminum and calcium in out-of-furnace refining of industrial silicon without affecting The invention relates to removing and reducing impurity elements iron and titanium in industrial silicon, belonging to the field of industrial silicon production and refining. Background technique [0002] In the production process of industrial silicon, some impurity elements in raw materials and fuels will be reduced into industrial silicon at high temperature, mainly including calcium, aluminum, titanium, iron, phosphorus, etc. Some downstream users of industrial silicon have strict requirements on the content of the above-mentioned impurities in finished products. Therefore, at present, most active elements such as calcium and...

Claims

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Application Information

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IPC IPC(8): C01B33/037
Inventor 龙潇罗文波陈发楼吕钧徐向军郑小宁龙绍檑王家贤
Owner GUIZHOU INST OF TECH
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