Pesticide micro-granule for spraying foliage in air, and preparation method and application of pesticide micro-granule
A microparticle and foliar spray technology, which is applied in the field of new pesticide formulations, can solve problems such as loss and pesticide deposition rate of less than 50%, and achieve the effect of overcoming evaporation and drift, optimizing spraying and operating parameters
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Embodiment 1
[0052] 0.5% methylamino abamectin benzoate emulsifiable microgranules: fully shear and mix the original drug containing 2.5 g methylamino abamectin benzoate and 10 g alkylphenol polyoxyethylene ether, About 37.5 g of water were slowly added under shear to form a microemulsion. 5g lignosulfonate, 5g acrylic acid-sulfonate copolymer, 15g long-chain polycarboxylate, 10g dodecyl sulfate, 5g sodium carboxymethyl cellulose, 100g urea, 50g potassium dihydrogen phosphate, 10g of soluble starch and 280g of kaolin were accurately weighed and added to a shearing kettle containing about 500g of water for shearing and mixing, and then into a sand mill for sand grinding. When the average particle size reached about 2 microns, it was transferred to the modulation kettle.
[0053] The microemulsion containing methylamino abamectin benzoate prepared above was added to the above preparation kettle under stirring conditions, sheared and mixed for about 10 minutes, and spray-dried and granulated....
Embodiment 2
[0056] 3% trioxystrobin-tebuconazole emulsifiable microgranules: fully shear and mix the original drug containing 5g trichostrobin and 10g tebuconazole, 20g alkylphenol polyoxyethylene ether and 10g N-methylpyrrolidone, evenly, About 55 g of water was slowly added under shear to form a microemulsion. 10g dodecyl sulfate, 5g sodium carboxymethyl cellulose, 100g urea, 50g potassium dihydrogen phosphate, 10g soluble starch, 280g kaolin were respectively accurately weighed and added to a shearing kettle filled with about 500g water, shearing and mixing. , and then into a sand mill for sand grinding, and when the average particle size reaches about 2 microns, spray drying and granulation are performed.
[0057]At the same time as the above spray-drying granulation, the microemulsion containing tristrobin and tebuconazole prepared above was sprayed onto the boiling microparticles in the spray-drying granulator, together with a 5% polyvinyl alcohol aqueous solution. Adjust and contr...
Embodiment 3
[0061] 0.3% dicamba emulsifiable microgranules: the original drug containing 3g dicamba and 30g lignosulfonate, 15g long-chain polycarboxylate, 15g sodium carboxymethyl cellulose, 10g soluble starch, 100g dodecyl Sodium sulfate and 800g of bentonite were respectively accurately weighed and added to a shearing kettle containing about 1000g of water, sheared and mixed, and then entered into a sand mill for sand grinding. When the average particle size reached about 2 microns, they were transferred to the modulation kettle.
[0062] Shear mixing for about 10 minutes and spray drying granulation. Adjust and control the spray drying operation parameters [specifically, refer to the prior art in the field of spray granulation technology, and those of ordinary skill in the art can realize it without paying creative work], control the granulation, the average particle size is 100 microns, and the granulation is 32 mesh (495 microns in turn). micron) and 325 mesh (47 micron) sieve, the ...
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