Micro-crosslinking viscosity-reducing mud-resistant polycarboxylic acid water reducer and preparation method thereof
A mud-resistant, polycarboxylic acid technology, applied in the field of concrete admixtures, can solve the problems of loss of workability, high viscosity of high-mud concrete, not easy to pump, loss of slump retention, etc., to achieve excellent construction performance, promote application and Promote and reduce the effect of water absorption and swelling
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Embodiment 1
[0031] 1.1 Raw materials (by weight)
[0032] 200 parts of unsaturated polyether macromonomer; 30 parts of unsaturated acid (anhydride) small monomer; 3 parts of unsaturated silane monomer; 5 parts of chain transfer agent; 15 parts of single-electron oxidant; 250 parts of deionized water.
[0033] In this embodiment, the unsaturated polyether macromonomer is methallyl polyoxyethylene ether (molecular weight is 2400);
[0034] The unsaturated acid (anhydride) small monomer is acrylic acid;
[0035] The unsaturated silane monomer is 3-methacrylamide-propyltrimethylsilane;
[0036] The chain transfer agent is mercaptoethanol;
[0037] The one-electron oxidizer is ceric ammonium nitrate.
[0038] 1.2 Preparation method
[0039] (1) take each raw material by proportioning;
[0040] (2) Configure liquid A and liquid B;
[0041] Mix 10 parts (by weight) of unsaturated acid (anhydride) small monomers, unsaturated silane monomers, chain transfer agent and 35 parts (by weight) of ...
Embodiment 2
[0047] The difference between this embodiment and Example 1 is: 6 parts of unsaturated silane monomers (by weight);
[0048] All the other are the same as Example 1, and obtain the finished product of micro-crosslinked viscosity-reducing anti-mud type polycarboxylic acid deionized water agent.
Embodiment 3
[0050] The difference between this embodiment and Example 1 is: 9 parts (by weight) of unsaturated silane monomer;
[0051] All the other are the same as Example 1, and obtain the finished product of micro-crosslinked viscosity-reducing anti-mud type polycarboxylic acid deionized water agent.
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