Process for producing solid particles, solid particles and use thereof
A technology of solid particles and inorganic solids, applied in chemical instruments and methods, improvement of process efficiency, silicon compounds, etc.
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[0104] Two mineral concentrates or concentrates (inorganic solids containing at least one alkali metal and / or alkaline earth metal) derived from lithium extraction and consisting essentially of spodumene, containing a) 5.0% by mass of Li 2 O and b) 7.0% by mass of Li 2 O, the calcination and leaching process (extraction) was carried out on a laboratory scale under the following conditions:
[0105] Calcination temperature: 1100°C
[0106] Calcination time: 1h
[0107] Baking temperature: 250℃
[0108] Baking time: 1h
[0109] h 2 SO 4 / Spodumene: 0.3
[0110] Water / spodumene: 3:1
[0111] Flushing solution / spodumene: 1:1
[0112] Extraction temperature: 90°C
[0113] Extraction time: 1h
[0114] After the above-mentioned extraction or leaching, two lithium-depleted residues and thus solid particles according to the invention are obtained, hereinafter referred to as TLR 5.0 and TLR 7.0 (TLR=Test Leach Residue). The following chemical, physical and mineralogical prope...
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