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Gel capable of stabilizing fragrant substances

A fragrance substance and gel technology, applied in the field of supramolecular gel, can solve the problems of incongruity, inconsistent release behavior, volatilization loss of fragrance components, etc., and achieve the effects of prolonging release time, lasting physiological sensation, and reducing release loss.

Active Publication Date: 2021-08-03
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] Although nicotine salts have been widely used in e-cigarette liquids, there are still the following main sensory problems in e-cigarettes containing nicotine salts: when nicotine salts are heated and decomposed to form free nicotine and delivered to the atomized vapor, puff-by-puff nicotine The release behavior is inconsistent with the release behavior of the aromatizing ingredients, and it is difficult to achieve the synergistic delivery of the key aromatizing ingredients and nicotine. While bringing nicotine physiological satisfaction, it cannot bring the matching characteristic fragrance, resulting in the interaction between nicotine and flavoring substances. The sensory sensations are strong and weak, covering each other or even repelling each other, especially for volatile characteristic aroma substances, because they cannot be released stably throughout the smoking process (usually the release amount gradually decreases mouth by mouth), this sense of incongruity especially obvious
Another common problem with e-cigarettes is that during the storage of e-liquid or pods, there will inevitably be a problem of volatilization and loss of flavor components. Even closed pods also have the problem of deterioration of flavor substances.
At present, although microcapsule technology can be used to encapsulate volatile aroma components, since microcapsules mostly use sugars such as cyclodextrin as wall materials, there will be a problem caused by the wall material adhering to the heating element at the heating temperature of the electronic cigarette. burnt smell and discomfort

Method used

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  • Gel capable of stabilizing fragrant substances
  • Gel capable of stabilizing fragrant substances
  • Gel capable of stabilizing fragrant substances

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0077] A method of preparing a gel that stabilizes the flavor substance, including the following steps:

[0078] Step 1, the preparation of the gelling agent: Press the racemic malic acid and nicotine to 2: 1 molar ratio, soluble in ethanol, respectively, racemic malic acid and dissolved ethanol mass ratio of 1 g: 28ml, nicotine and dissolution The ethanol mass ratio is 1 g: 210 mL, stirred at room temperature to completely dissolve, each obtained racemic malic acid solution and nicotine solution, and then thoroughly mixed the above two solutions to obtain a mixed liquid to warming the mixture To reflux, the reaction was 30 min, 190 mbar, and evaporated, then the evaporated product was dried at 36 ° C for 1.5 h, resulting in a racemic maline glycodehydrogen gelling agent;

[0079] Step 2, the preparation of the gel:

[0080] The fragrant substance was dissolved in 1,2-propanediol to obtain a flavor solvent, and the volume ratio of fragrance and 1,2-propylene glycol mass was 1 g: 2...

Embodiment 2

[0084] This example provides the application of a carrier super molecular gel prepared in the first embodiment of the present invention in a heating cigarette

[0085] The Ni Dated Salt Syrotic Molecular Gel can separately apply a single gel or different types of mixed gels in the manufacturing process of reacting cigarette and exciting pulp to heat the cigarette.

[0086] Papermaking method heating the cigarette use to make tobacco:

[0087]Method 1: A quantitative cosmetic (1,2-propanediol, glycerol or two proportible mixtures) is added to the preparation of the carrier super molecular gel, and the quality of the super molecular gel and the quality of the smoke. The ratio is 5: 1, warmed to 85 ° C, gel melting into a sol, uniformly mixed, forming a mixed coating liquid containing a molten gel and a smoke agent, spraying a mixed coating liquid to paper The preparative tobacco tablet is made. Reproduction tobacco the above mixed coating liquid is applied to room temperature, which...

Embodiment 3

[0099] This example provides the application of the carried abstentive ultra molecular gel prepared in Example 1 in the electronic smoke.

[0100] The Niurota salt hypermor gel can be applied to the electronic cigarette in two ways and can be used in accordance with the actual use of a single gel or different types of mixed gels.

[0101] Method 1: After 24-36 h, a hemolecular gel prepared in an oven at a 40 ° C oven 24-36 h, after the drying gel is ground into a uniform microparticle, and a certain amount of electronic smoke is added to a certain proportion. The mixture is thoroughly stirred in the changering agent, and the hybrid agent is a mixed solvent of glycerol and 1,2-propylene glycol 1.5: 1 (volume ratio), and the proportion of incense ultrasonic gel and the hairy agent mass is 1: 120, and after mixing is uniform. Fragrant gel-containing cosmetic or as an excipients were added to the finished tofonic mixed uniform mixed uniform as a metallogenic gel.

[0102] Smoky in the...

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Abstract

The invention belongs to the field of supramolecular gel, and particularly relates to gel capable of stabilizing fragrant substances. The gel comprises a racemic malic acid nicotine salt gelling agent, and a flavor substance and an organic solvent which are dispersed in the racemic malic acid nicotine salt gelling agent. The nicotine salt gel is used as a carrier of the flavor substance and a smoke agent, the requirement for the loading function of the reconstituted tobacco base is lowered, and use of a large amount of loading filler is reduced. For the reconstituted tobacco by the thick slurry method, even if relatively high moisture needs to be removed during drying, the loss of the fragrant substance and the smoke agent can be effectively avoided while the moisture is removed by adopting measures such as low-temperature multi-stage drying and the like due to the fact that the fragrant substance and the smoke agent are fixed in the gel.

Description

Technical field [0001] The present invention belongs to the field of ultra-molecular gels, and more particularly to a gel that stabilizes the flavor substance. Background technique [0002] Alkaline nicotine can react with the carboxyl group of organic acid to generate nicotinuclearboxylates. Nicotine comprises a pyridine ring and a pyrrole ring, wherein the pyrrolei nitrogen is more basic, which is tended to react with a carboxylate of the carboxylic acid to generate nicotine salts, and the alkaline of pyridine is weak, and it is substantially ionized effect. Non-covalent effects such as hydrogen bonds are combined with carboxylic acids. Naturally containing a variety of carboxylic acid nuron salts in the tobacco leaves, nicotine salts can be divided into 1: 1 acid base ratio, 2: 1 acid base ratio, 3: 1 acid base ratio, 3: 1 acid base ratio, 3: 1 acid base ratio, 3: 1 acid base ratio, 3: 1 acid base ratio Among them, common nicotinarboxylates include tartaric acid nicotinium, ra...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B3/14A24B15/26A24B15/28A24B15/167
CPCA24B3/14A24B15/26A24B15/28A24B15/167
Inventor 韩熠赵伟巩效伟杨柳朱东来吕茜洪鎏尚善斋段沅杏秦云华陈永宽
Owner CHINA TOBACCO YUNNAN IND
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