Production and preparation method of calculus bovis factitius-venenum bufonis granule, prepared calculus bovis factitius-venenum bufonis granule and application of calculus bovis factitius-venenum bufonis granule
A technology of granule and bovine toad, which is applied in the directions of non-active ingredient medical preparations, medical preparations containing active ingredients, and pharmaceutical formulas, etc. problems, to improve the efficacy of drugs, improve the dispersion effect, improve the effect of palatability
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Embodiment 1
[0019] Embodiment 1 Preparation of Niutoad granules of the present invention
[0020] (1) Take by weighing 4g artificial bezoar, 2g toad venom, 2g borneol, 1000g scutellaria baicalensis, 200g licorice for later use;
[0021] (2) Prepare a citric acid buffer solution with a pH of 3.5: 0.1mol / L citric acid solution, take 21.01g of citric acid, add 1000ml of purified water, dissolve, shake well, 0.1mol / L sodium citrate solution, take sodium citrate 29.41g, add 1000ml of purified water, dissolve, shake well, the volume ratio of the two is 15.5:4.5, mix well;
[0022] (3) Add the artificial bezoar and toad venom taken in step (1) into 100 parts by weight of fresh milk and grind evenly, then filter, and the filtrate is for subsequent use;
[0023] (4) Take 7g of phospholipids and 3g of cholesterol, add 50ml of absolute ethanol, stir in a water bath at 70°C to dissolve and disperse the ethanol, add 100ml of citric acid buffer at the same temperature after film formation, stir in a w...
Embodiment 2
[0028] Embodiment 2 The preparation of another bovine toad granule of the present invention
[0029] (1) Take by weighing 4g artificial bezoar, 2g toad venom, 2g borneol, 1000g scutellaria baicalensis, 200g licorice for later use;
[0030](2) Prepare a citric acid buffer solution with a pH of 5.0: 0.1mol / L citric acid solution, take 21.01g of citric acid, add 1000ml of purified water, dissolve, shake well, 0.1mol / L sodium citrate solution, take sodium citrate 29.41g, add 1000ml of purified water, dissolve, shake well, the volume ratio of the two is 8.2:11.8;
[0031] (3) Add the artificial bezoar and toad venom taken in step (1) into 100 parts by weight of fresh milk and grind evenly, then filter, and the filtrate is for subsequent use;
[0032] (4) Take 7g of phospholipids and 3g of cholesterol, add 50ml of absolute ethanol, stir in a water bath at 73°C to dissolve and disperse the ethanol, add 100ml of citric acid buffer at the same temperature after film formation, stir in...
Embodiment 3
[0037] Embodiment 3 The preparation of another bovine toad granule of the present invention
[0038] (1) Take by weighing 4g artificial bezoar, 2g toad venom, 2g borneol, 1000g scutellaria baicalensis, 200g licorice for later use;
[0039] (2) Prepare a citric acid buffer solution with a pH of 6.0: 0.1mol / L citric acid solution, take 21.01g of citric acid, add 1000ml of purified water, dissolve, shake well, 0.1mol / L sodium citrate solution, take sodium citrate 29.41g, add 1000ml of purified water, dissolve, shake well, the volume ratio of the two is 3.8:16.2;
[0040] (3) Add the artificial bezoar and toad venom taken in step (1) into 100 parts by weight of fresh milk and grind evenly, then filter, and the filtrate is for subsequent use;
[0041] (4) Take 7g of phospholipids and 3g of cholesterol, add 50ml of absolute ethanol, stir in a water bath at 75°C to dissolve and disperse the ethanol, add 100ml of citric acid buffer at the same temperature after film formation, stir i...
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