A method of dividing the fresh cut flower water in Tangyu Pu
A measurement method and fresh-cut flower technology, applied in the direction of measuring devices, analysis materials, test sample preparation, etc., to achieve the effect of optimizing fresh-keeping technology, improving the ratio of preservatives, and satisfying real-time feedback
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Embodiment 1
[0038] Example 1: Moisture content during the opening process of gladiolus florets
[0039] ⑴ parameter debugging.
[0040] The first step: Due to the requirements of the uniformity of the magnetic field of the instrument, the height of the sample must be less than the set Fov value of the field of view. The coil diameter of the NMI20 low-field nuclear magnetic resonance detector used in the test is 15mm. In order to ensure the accuracy of the sample detection results, the range of the sample loading height should not exceed 2.5cm. During the actual test, it was found that the cut flower has a high filling value, and it is difficult to compress to the detection height when the sample size is higher than 0.6g. So cut the petal sample into 1cm 2 Small piece, take 0.5g and put it into a dry and clean NMR sample tube with a diameter of 15mm and seal it.
[0041]The second step: use a single 90-degree radio frequency pulse to excite the sample, and receive the hard pulse FID sig...
Embodiment 2
[0050] Example 2: Moisture status of different organs and tissues of gladiolus cut flowers and their postharvest distribution changes
[0051] ⑴ sample collection and determination. Cut the bract and petal samples into about 1cm 2 Take about 0.5g of each small piece, cut the stem section into a height of no more than 2cm, and put it into a dry and clean NMR sample tube with a diameter of 15mm and seal it. Through the CPMG sequence, the first point signal value is extracted, and the NMR signal amplitude and transverse relaxation time T2 of each relaxation component are obtained by inversion, and the sample data is collected.
[0052] ⑵ data analysis. The characteristic peaks of gladiolus cut flowers were obtained, and the NMR signals with T2 values of 1 to 10, 10 to 100, and 100 to 10000 ms were analyzed as bound water (T21), difficult-to-flow water (T22) and free water (T23). Amplitude and T2 analysis of sample water content. There are differences in the NMR signal ampli...
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Abstract
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