Preparation method of high-purity aluminum oxide ceramic substrate
A high-purity alumina and ceramic substrate technology, applied in the field of ceramic materials, can solve the problems of poor controllability of sintering process, poor controllability of sintering shrinkage, large forming defects of high-purity alumina ceramic substrate, etc. Good controllability, widening sintering range, small deformation effect
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Embodiment 1
[0030] A method for preparing a high-purity alumina ceramic substrate in this embodiment includes the following steps:
[0031] S1. Slurry preparation: put 99 parts by weight of high-purity alumina powder and 1 part by weight of sintering aid into a ball mill, use water as a solvent, add a water-soluble dispersant, grind and mix to obtain Ceramic slurry with high solid content, good fluidity and uniform suspension;
[0032] S2. Molding: Place the ceramic slurry in a closed container after vacuum defoaming, take the ceramic slurry corresponding to the weight required by the mold and put it into the slurry tank, add catalyst and initiator, stir evenly, and connect the slurry tank to the air Source, open the air source to apply pressure to the ceramic slurry in the slurry tank to control the ceramic slurry in the slurry tank through the connecting pipe with a control valve connecting the slurry tank and the grouting port at the bottom of the mold at a rate of 340ml / min The injec...
Embodiment 2
[0040] A method for preparing a high-purity alumina ceramic substrate in this embodiment includes the following steps:
[0041] S1. Slurry preparation: put 99.3 parts by weight of high-purity alumina powder and 0.7 parts by weight of sintering aid into a ball mill, use water as a solvent, add a water-soluble dispersant, grind and mix to obtain Ceramic slurry with high solid content, good fluidity and uniform suspension;
[0042] S2. Molding: Place the ceramic slurry in a closed container after vacuum defoaming, take the ceramic slurry corresponding to the weight required by the mold and put it into the slurry tank, add catalyst and initiator, stir evenly, and connect the slurry tank to the air Source, open the air source to apply pressure to the ceramic slurry in the slurry tank to control the ceramic slurry in the slurry tank through the connecting pipe with a control valve connecting the slurry tank and the grouting port at the bottom of the mold at a rate of 450ml / min The ...
Embodiment 3
[0050] A method for preparing a high-purity alumina ceramic substrate in this embodiment includes the following steps:
[0051] S1. Slurry preparation: put 99.5 parts by weight of high-purity alumina powder and 0.5 parts by weight of sintering aid into a ball mill, use water as a solvent, add a water-soluble dispersant, grind and mix to obtain Ceramic slurry with high solid content, good fluidity and uniform suspension;
[0052] S2. Molding: Place the ceramic slurry in a closed container after vacuum defoaming, take the ceramic slurry corresponding to the weight required by the mold and put it into the slurry tank, add catalyst and initiator, stir evenly, and connect the slurry tank to the air Source, open the air source to apply pressure to the ceramic slurry in the slurry tank to control the ceramic slurry in the slurry tank through the connecting pipe with a control valve connecting the slurry tank and the grouting port at the bottom of the mold at a rate of 580ml / min The ...
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