A kind of cigarette filter additive material and its preparation method and application
A cigarette filter tip and technology for adding materials, applied in the directions of application, separation method, e-liquid filter, etc., can solve the problems of reducing the release of crotonaldehyde in cigarettes, being unfavorable for large-scale production, reducing crotonaldehyde in smoke, etc., and improving the choice High adsorption capacity, favorable adsorption, low cost effect
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[0021] An aspect of the embodiments of the present invention provides a method for preparing a cigarette filter additive material, which includes:
[0022] Mix surfactant, activated carbon, and water evenly to obtain surfactant-modified activated carbon;
[0023] And, uniformly mix the surfactant-modified activated carbon, attapulgite, pregelatinized starch and binder solution to obtain attapulgite-activated carbon composite material, and then granulate to obtain attapulgite-activated carbon composite material Particles, that is, to obtain cigarette filter additive materials.
[0024] In some more specific embodiments, the method includes: dissolving the binder in a binder solvent to obtain the binder solution.
[0025] Further, the binder solvent is an aqueous solution, especially preferably a 1-5 wt% aqueous solution of acetic acid, an aqueous solution above 98°C, or an aqueous solution above 95°C.
[0026] Furthermore, the solvent for dissolving the chitosan is an aqueous...
Embodiment 1
[0059] A cigarette filter additive material for selectively reducing the adsorption of crotonaldehyde in mainstream cigarette smoke, including the following components: 200g attapulgite, 300g activated carbon, 400g pregelatinized starch, 3g cetyltrimethylammonium bromide, 8g Chitosan, 800g contains 1% acetic acid aqueous solution in mass fraction.
[0060] The preparation method of the cigarette filter additive material that adsorbs crotonaldehyde of the present embodiment comprises the following steps:
[0061] (1) 3g cetyltrimethylammonium bromide is dissolved in deionized water to form cetyltrimethylammonium bromide solution, wherein the concentration of cetyltrimethylammonium bromide solution is 100mg / L, then add 300g of activated carbon to the hexadecyltrimethylammonium bromide solution, then stir at 30°C for 3h, after the adsorption equilibrium, filter the activated carbon, rinse with deionized water, and dry to obtain the modified surfactant Activated carbon;
[0062...
Embodiment 2
[0067] A cigarette filter additive material for selectively reducing the adsorption of crotonaldehyde in cigarette mainstream smoke, including the following components: 300g attapulgite, 100g activated carbon, 600g pregelatinized starch, 6g tetradecyltrimethylammonium bromide, 5g Carboxymethylcellulose.
[0068] The preparation method of the cigarette filter additive material that adsorbs crotonaldehyde of the present embodiment comprises the following steps:
[0069] (1) 6g tetradecyltrimethylammonium bromide is dissolved in deionized water to form tetradecyltrimethylammonium bromide solution, wherein the concentration of tetradecyltrimethylammonium bromide solution is 50mg / L, then add 100g of activated carbon to tetradecyltrimethylammonium bromide solution, and then stir at 20°C for 6h. Activated carbon;
[0070] (2) The carboxymethyl cellulose of 5g is dissolved in 1000g water to form carboxymethyl cellulose aqueous solution;
[0071] (3) the attapulgite powder of 300g,...
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