Preparation method of high-transmittance shielding film based on silver nanowires
A technology of silver nanowires and nanowires, which is used in the manufacture of conductive/semiconductive layer equipment, magnetic field/electric field shielding, cable/conductor manufacturing, etc. It can solve the problem of insufficient light transmission and shielding properties of high-transparency shielding films Excellent light transmittance, low square resistance and good shielding effect
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Embodiment 1
[0021] A method for preparing a high-transparency shielding film based on silver nanowires, comprising the following steps:
[0022] Step 1. Place the silver nanowires in a low-temperature plasma processor for 15 minutes, add the treated silver nanowires into the ammonium sulfide solution for irradiation and stirring reaction, separate solid and liquid, and wash to obtain silver sulfide-silver composite structure nano line; the atmosphere of the low-temperature plasma processor is argon; the frequency of the low-temperature plasma processor is 65KHz, the power is 80W, and the pressure of the atmosphere is 70Pa; Gamma ray irradiation reaction 120min; The concentration of described ammonium sulfide solution is 0.5mmol / L; The molar ratio of described silver nanowire and ammonium sulfide 2:1;
[0023] Step 2. After mixing the silver nanowires, the amphiphilic solvent and the non-polar solvent, the dispersion A is obtained; after the silver telluride nanowires, the amphiphilic solv...
Embodiment 2
[0026] A method for preparing a high-transparency shielding film based on silver nanowires, comprising the following steps:
[0027] Step 1. Place the silver nanowires in a low-temperature plasma processor for 15 minutes, add the treated silver nanowires into the ammonium sulfide solution for irradiation and stirring reaction, separate solid and liquid, and wash to obtain silver sulfide-silver composite structure nano line; the atmosphere of the low-temperature plasma processor is argon; the frequency of the low-temperature plasma processor is 75KHz, the power is 100W, and the pressure of the atmosphere is 65Pa; Gamma ray irradiation reaction 90min; The concentration of described ammonium sulfide solution is 0.8mmol / L; The molar ratio of described silver nanowire and ammonium sulfide 3:1;
[0028]Step 2. After mixing the silver nanowires, the amphiphilic solvent and the non-polar solvent, the dispersion A is obtained; after the silver telluride nanowires, the amphiphilic solve...
Embodiment 3
[0031] A method for preparing a high-transparency shielding film based on silver nanowires, comprising the following steps:
[0032] Step 1. Place the silver nanowires in a low-temperature plasma processor for 12 minutes, add the treated silver nanowires into the ammonium sulfide solution for irradiation and stirring reaction, separate solid and liquid, and wash to obtain silver sulfide-silver composite structure nano line; the atmosphere of the low-temperature plasma processor is argon; the frequency of the low-temperature plasma processor is 50KHz, the power is 60W, and the pressure of the atmosphere is 45Pa; Gamma ray irradiation reaction 100min; The concentration of described ammonium sulfide solution is 0.6mmol / L; The molar ratio of described silver nanowire and ammonium sulfide is 1:1;
[0033] Step 2. After mixing the silver nanowires, the amphiphilic solvent and the non-polar solvent, the dispersion A is obtained; after the silver telluride nanowires, the amphiphilic s...
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