Process for preparing metal-chelate retarder by sol-gel method
A retarder and chelate technology, which is applied in the field of preparation of new retarders, can solve the problems of long production cycle, short production cycle and complicated preparation of retarders, and achieve adjustable thickening time and short production cycle , the effect of simple operation
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Embodiment 1
[0026] A kind of technology that utilizes sol-gel method to prepare metal-chelate type retarder, specifically comprises the following steps:
[0027] Calcium nitrate tetrahydrate (Ca(NO 3 ) 2 4H 2 O) 80g, aluminum nitrate nonahydrate (Al(NO 3 ) 3 9H 2 O) 20g, iron nitrate nonahydrate (Fe(NO 3 ) 3 9H 2 (2) 10g, then add 50ml deionized water, place on magnetic stirrer and stir 50min, make it mix uniformly, obtain mixed solution A; Weigh citric acid monohydrate (C 6 h 8 o 7 ·H 2 O) 40g is added to the mixed solution A, placed in a water bath at 80°C and stirred to obtain a light yellow solution B; 5 g of ethylene glycol is added successively to the light yellow solution B to undergo an esterification reaction, which lasts for 12 hours to obtain a metal-chelate compound type retarder.
Embodiment 2
[0029] A kind of technology that utilizes sol-gel method to prepare metal-chelate type retarder, specifically comprises the following steps:
[0030] Calcium nitrate tetrahydrate (Ca(NO 3 ) 2 4H 2 O) 90g, aluminum nitrate nonahydrate (Al(NO 3 ) 3 9H 2 O) 30g, iron nitrate nonahydrate (Fe(NO 3 ) 3 9H 2 (0) 10g, then add 60ml of deionized water, place on a magnetic stirrer and stir for 50min, make it mix evenly, and obtain mixed solution A; weigh 30g of gluconic acid and add in mixed solution A, place in 80 ℃ water bath and stir to obtain light Yellow solution B: Add 10 g of glycerol to the light yellow solution B in sequence to undergo esterification reaction, which lasts for 12 hours to obtain a metal-chelate type retarder.
Embodiment 3
[0032] A kind of technology that utilizes sol-gel method to prepare metal-chelate type retarder, specifically comprises the following steps:
[0033] Calcium nitrate tetrahydrate (Ca(NO 3 ) 2 4H 2 O) 120g, aluminum nitrate nonahydrate (Al(NO 3 ) 3 9H 2 O) 40g, iron nitrate nonahydrate (Fe(NO 3 ) 3 9H 2 (2) 15g, then add 70ml deionized water, place on magnetic stirrer and stir 60min, make it mix uniformly, obtain mixed solution A; Weigh citric acid monohydrate (C 6 h 8 o 7 ·H 2 O) 50g was added to the mixed solution A, placed in a 60°C water bath and stirred to obtain a light yellow solution B; 20g of glycerol was added to the light yellow solution B to undergo an esterification reaction, and the temperature of the water bath was adjusted to 80°C after one hour , continued for 15 hours to obtain a metal-chelate retarder.
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