Decontamination self-cleaning insulator protective agent and preparation method thereof
A self-cleaning, insulator technology, used in biocide-containing paints, antifouling/underwater coatings, coatings, etc. Enhanced adhesion and performance durability, excellent cleaning and detergency, and increased densification effects
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[0045] According to the decontamination and self-cleaning insulator protective agent provided by the present invention, the surface treatment agent includes 15-35 parts of hydrophobic nanoparticles, preferably 20-30 parts by weight. The hydrophobic nano-particles in the present invention are hydrophobic nano-silica powder, the particle size of the hydrophobic nano-silica powder is 50-200nm, and the preparation method of the hydrophobic nano-silica powder includes the following steps : Mixing nano-silica powder, bis-(γ-triethoxysilylpropyl) tetrasulfide, water, azobisisobutyronitrile and ethanol, the nano-silica powder, bis- The mass ratio of (γ-triethoxysilylpropyl) tetrasulfide, water, azobisisobutyronitrile and ethanol is (4-8): (2-5): (0.5-1): (0.05 -0.5): (3-6), after stirring for 3-6h in a reaction kettle at 50-120℃, mixture one is obtained, and the mixture is naturally cooled to room temperature, and the above mixture one is extracted at 50-80℃ using a Soxhlet extractor. ...
Embodiment 1
[0050] 1) The configuration of the mixed solvent: stir and disperse 5 parts of isopropanol, 20 parts of 120# gasoline, 56 parts of trifluorotrichloroethane and 10 parts of ethanol to obtain a mixed solvent;
[0051] 2) The configuration of the primer: add 3 parts of hydrogen-containing silicone oil to 89 parts of the above-mentioned mixed solvent, and then add 8 parts of micron particles at a speed of 1500 rpm and continue to disperse at a high speed for 15 minutes to obtain the primer ;
[0052] 3) The configuration of the surface treatment agent: stir and mix 15 parts of low surface energy resin with 55 parts of ethyl acetate, and then add 30 parts of hydrophobic nanoparticles at a speed of 5000 rpm to continue high-speed dispersion for 25 minutes to obtain the surface treatment agent ;
[0053] The active hydrogen content of the hydrogen-containing silicone oil in the present invention is 0.35%, and the viscosity is 110 mPa·s,
[0054] The hydrophobic nano-particles are hydrophobi...
Embodiment 2
[0056] 1) The configuration of the mixed solvent: 15 parts of isopropanol, 25 parts of 120# gasoline, 52 parts of trifluorotrichloroethane and 8 parts of ethanol are stirred and dispersed uniformly to obtain a mixed solvent;
[0057] 2) The configuration of the primer: add 6 parts of hydrogen-containing silicone oil to 82 parts of the above mixed solvent, and then add 12 parts of micron particles at 3000 rpm and continue to disperse at high speed for 20 minutes to obtain the primer ;
[0058] 3) The configuration of the surface treatment agent: stir and mix 10 parts of low surface energy resin with 65 parts of ethyl acetate, then add 25 parts of hydrophobic nanoparticles at 3000 rpm and continue to disperse at high speed for 20 minutes to obtain the surface treatment agent ;
[0059] The hydrogen-containing silicone oil in the present invention has an active hydrogen content of 0.6% and a viscosity of 580 mPa·s; the hydrophobic nanoparticles include hydrophobic nano silica with part...
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