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Low-foam low-quantity glufosinate-ammonium and glyphosate surfactant and preparation process thereof

A technology of surfactant and preparation process, which is applied in the direction of herbicides, algicides, biocides, biocides, etc., can solve the problems of increasing the difficulty of cleaning and high foaming, and achieves easy processing and preparation, simple production process, and reduced The effect of cost of use

Inactive Publication Date: 2019-11-22
南京拓际生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The object of the present invention is to provide a low-foaming low-volume type glufosinate-ammonium and glyphosate surfactant and its preparation process, to solve the problem of high foaming when the active agent produced above is used, which increases the difficulty of cleaning

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] The following substances are taken by weight: 18% cocamidopropyl ammonium oxide, 18% nonylphenol ethoxylates, 15% dibenzyl biphenyl ethoxylates, 10% alkylphenylene ether sulfonates, 10% Alkylphenol polyether, 5% JFC-1, 2% citric acid, and two parts 11% deionized water.

[0021] Add 11% deionized water to the reaction kettle, add weighed 18% cocamidopropyl ammonium oxide, 18% nonylphenol polyoxyethylene ether and 15% dibenzyl biphenyl polyoxyethylene ether, stir and heat to 60°C, the stirring time is 5m, the stirring speed is 2000r / min; then add 10% alkyl phenylene ether sulfonate, 10% alkylphenol polyether and 5% JFC-1, the stirring speed is adjusted to 1000r / min, at the same time The heating temperature was adjusted to 70°C; after stirring evenly, 2% citric acid was added to adjust the pH, 11% deionized water was added, and the stirring speed was adjusted to 3000r / min.

[0022] Carry out viscosity measurement to the prepared low-foam low-volume type glufosinate-ammoni...

Embodiment 2

[0035] Take the following materials by weight: 18% lauryl amidopropyl dimethyl ammonium oxide, 18% nonylphenol ethoxylates, 15% stearyl ethoxylates, 10% naphthalenesulfonate polymer, 10 % alkylphenylene ether sulfonate, 5% JFC-2, 2% citric acid, and two parts 11% deionized water.

[0036] Add 11% deionized water to the reactor, add weighed 18% lauryl amidopropyl dimethyl ammonium oxide, 18% nonylphenol polyoxyethylene ether and 15% stearyl polyoxyethylene ether, stir Heating to 60°C, the stirring time is 5m, and the stirring speed is 2000r / min; then add 10% naphthalene sulfonate polymer, alkyl phenylene ether sulfonate and 5% JFC-2, and adjust the stirring speed to 1000r / min, At the same time, the heating temperature was adjusted to 70°C; after stirring evenly, 2% citric acid was added to adjust the pH, 11% deionized water was added, and the stirring speed was adjusted to 3000r / min.

[0037] According to the test method of Example 1, the viscosity of the low-foaming and low-v...

Embodiment 3

[0039] Take the following substances by weight: 18% cetyl dimethyl amine oxide, 18% octylphenol ethoxylate, 15% stearyl polyoxyethylene ether, 10% alkylphenol polyether phosphate, Alkyl sulfates, 5% AEO-5, 2% citric acid, and two parts 11% deionized water.

[0040] Add 11% deionized water to the reaction kettle, add weighed 18% cetyl dimethyl amine oxide, 18% octylphenol polyoxyethylene ether and 15% stearyl polyoxyethylene ether, stir Heating to 60°C, the stirring time is 5m, and the stirring speed is 2000r / min; then add 10% alkylphenol polyether phosphate, alkyl sulfate and 5% JFC, the stirring speed is adjusted to 1000r / min, and the heating temperature is adjusted at the same time 70°C; after stirring evenly, add 2% citric acid to adjust the pH, add 11% deionized water, and adjust the stirring speed to 3000r / min.

[0041] According to the test method of Example 1, the viscosity of the low-foaming and low-volume glufosinate-ammonium glyphosate surfactant prepared by this fo...

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Abstract

The invention discloses a low-foam low-quantity glufosinate-ammonium and glyphosate surfactant. The surfactant comprises the following components in percentage by weight: 10-30% of ammonium oxide, 10-30% of the surfactant, 1%-20% of dispersing agent is, 1%-20% of wetting agent, 0.1%-10% of the penetrant0.1%-10% of pH regulator and the balance of deionized water, wherein the ammonium oxide is a combination of one or more of lauramidopropyl dimethyl ammonium oxide, cocamidopropylamine oxide, dodecyl dimethyl amine oxide, tetradecyl dimethyl amine oxide, hexadecyl dimethyl amine oxide, dodecyl dihydroxyethyl amine oxide, tetradecyl dihydroxyethyl amine oxide, octadecyl dihydroxyethyl amine oxide and octadecanamide propyl amine oxide.

Description

technical field [0001] The invention relates to the technical field of pesticide preparation, in particular to a low-foaming and low-volume glufosinate-ammonium and glyphosate surfactant and a preparation process thereof. Background technique [0002] Glyphosate is the most widely used herbicide in the world. It is non-flammable, non-explosive, and stable at room temperature. It is a non-selective and non-residual herbicide. Glufosinate-ammonium is a broad-spectrum contact herbicide with weak systemic effect. The herbicide has the characteristics of high efficiency, low toxicity and easy degradation. Due to the difficulty of synthesis, the market price of glufosinate-ammonium is relatively high. These two herbicides are quite different, especially in their distinct mechanisms of action. Glufosinate-ammonium is a glutamine synthetase (GS) inhibitor, which kills weeds by inhibiting this enzyme; unlike glyphosate that kills roots, glufosinate-ammonium kills leaves first, and...

Claims

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Application Information

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IPC IPC(8): A01N25/30A01N57/20A01P13/00
CPCA01N25/30A01N57/20
Inventor 何华雄
Owner 南京拓际生物科技有限公司
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