Graphene-based additive for PVC floor and preparation method thereof
A graphene-based and additive technology, which is applied in the field of graphene-based additives for PVC flooring and its preparation, can solve the problems of poor thermal conductivity, inconvenient installation, complex structure and the like, and achieves convenient production, low cost and simple preparation method. Effect
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Embodiment 1
[0038] The concrete steps of preparation are:
[0039] Step 1, according to the weight ratio of graphene with a particle size of 5 μm, titanium dioxide hydrosol with a concentration of 10%, and water at a weight ratio of 25:1:50, mix the three and stir for 15 minutes; wherein, graphene is a redox method The particle diameter of the prepared graphene powder is the lateral dimension, and the particle diameter of the titanium dioxide in the titanium dioxide hydrosol is 5 nm, and the graphene coated with the titanium dioxide hydrosol is obtained.
[0040] Step 2, vacuum-drying the graphene coated with the titanium dioxide hydrosol at 100° C. for 120 minutes; wherein, the vacuum degree during vacuum drying is 133 Pa, to obtain a composite graphene coated with 5 nm-thick titanium dioxide particles outside the graphene.
[0041] Step 3, according to the weight ratio of composite graphene, chlorinated polyethylene with a particle size of 400 μm, and titanate coupling agent of 100:1:5,...
Embodiment 2
[0043] The concrete steps of preparation are:
[0044] Step 1, according to the ratio of graphene with a particle size of 9 μm, titanium dioxide hydrosol with a concentration of 13%, and water at a weight ratio of 25:13:39, mix the three and stir for 26 minutes; wherein, graphene is a redox method The particle diameter of the prepared graphene powder is the lateral dimension, the particle diameter of the titanium dioxide in the titanium dioxide hydrosol is 16nm, and the graphene coated with the titanium dioxide hydrosol is obtained.
[0045] Step 2, place the graphene coated with titanium dioxide hydrosol at 113° C. for 97 minutes in vacuum; wherein, the vacuum degree during vacuum drying is 130 Pa, and obtain a composite graphene in which graphene is coated with titanium dioxide particles with a thickness of 28 nm.
[0046] Step 3, according to the weight ratio of composite graphene, chlorinated polyethylene with a particle size of 500 μm, and titanate coupling agent of 100:8...
Embodiment 3
[0048] The concrete steps of preparation are:
[0049] Step 1, according to the ratio of graphene with a particle size of 13 μm, titanium dioxide hydrosol with a concentration of 17%, and water at a weight ratio of 25:25:28, mix the three and stir for 38 minutes; wherein, graphene is a redox method The particle diameter of the prepared graphene powder is the lateral dimension, the particle diameter of the titanium dioxide in the titanium dioxide hydrosol is 28nm, and the graphene coated with the titanium dioxide hydrosol is obtained.
[0050] In step 2, the graphene coated with the titanium dioxide hydrosol was vacuum-dried at 125° C. for 75 minutes; wherein, the vacuum degree during vacuum drying was 123 Pa to obtain a composite graphene coated with 56 nm-thick titanium dioxide particles outside the graphene.
[0051] Step 3, according to the weight ratio of composite graphene, chlorinated polyethylene with a particle size of 600 μm, and titanate coupling agent of 100:16:2.8,...
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