Intelligent temperature regulation sentry box with thermal insulating and energy saving functions
A kind of sentry box and intelligent technology, which is applied in the field of intelligent temperature-regulating booths to achieve the effect of high thermal insulation and energy saving, broad application prospects, high efficiency, thermal insulation and energy saving.
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Embodiment 1
[0032] Take 3.0g Cs 0.32 WO 3 Disperse the powder in 100mL absolute ethanol, add 1.0g KH-570 and 2.5g tungsten chloride sol with a molar concentration of 0.25mol / L, stir magnetically for 2.5h, let it stand for 1.5h, centrifuge to precipitate, and calcinate at 350°C to obtain WO 3 Coated M x WO 3 / WO 3 Composite particles; the M x WO 3 / WO 3 Composite particles were dispersed in 70mL isopropanol, 1.0g polyvinyl alcohol, 3.0gV 2 o 5 and 4.1g oxalic acid, magnetically stirred at 50°C for 2.5h to obtain M x WO 3 / WO 3 / V 2 o 5 The reaction solution was reacted at 240°C for 12 hours, and M was obtained after washing with water, alcohol and centrifugal drying. x WO 3 / WO 3 / VO 2 particle. Take 0.3g of the above-mentioned particles and disperse them in 10wt% PVA solution, and coat a film on the glass surface. After testing, the transmittance of visible light and near-infrared is 55% and 20%, respectively.
Embodiment 2
[0034] Take 3.5g Cs 0.32 WO 3 Disperse the powder in 60mL of absolute ethanol, add 1.0g KH-570 and 1.8g tungsten chloride sol with a molar concentration of 0.25mol / L, stir magnetically for 2.5h, let it stand for 1.5h, centrifuge to precipitate, and calcined at 450°C to obtain WO 3 Coated Cs 0.32 WO 3 / WO 3 Composite particles; the Cs 0.32 WO 3 / WO 3 Composite particles were dispersed in 70mL isopropanol, 1.0g polyethylene glycol, 2.0gV 2 o 5 and 4.1g oxalic acid, magnetically stirred at 50°C for 2.5h to obtain Cs 0.32 WO 3 / WO 3 / V 2 o 5 The reaction solution was reacted at 240°C for 12 hours, and Cs was obtained after washing with water, alcohol and centrifugal drying. 0.32 WO 3 / WO 3 / VO 2 particle. Take 0.3g of the above-mentioned particles and disperse them in 10wt% PVA solution, and coat a film on the glass surface. After testing, the transmittances of visible light and near-infrared are 70% and 10%, respectively.
Embodiment 3
[0036] Take 2.5g Cs 0.32 WO 3 Disperse the powder in 60mL of absolute ethanol, add 0.8g KH-570 and 2.5g tungsten chloride sol with a molar concentration of 0.28mol / L, stir magnetically for 2.5h, let stand for 1.5h, centrifuge to precipitate, and calcined at 450°C to obtain WO 3 Coated Cs 0.32 WO 3 / WO 3 Composite particles; the Cs 0.32 WO 3 / WO 3 Composite particles were dispersed in 70mL isopropanol, 1.0g polyvinylpyrrolidone, 3.0gV 2 o 5 and 5.6g oxalic acid, magnetically stirred at 50°C for 2.5h to obtain Cs 0.32 WO 3 / WO 3 / V 2 o 5 The reaction solution was reacted at 240°C for 12 hours, and Cs was obtained after washing with water, alcohol and centrifugal drying. 0.32 WO 3 / WO 3 / VO 2 particle. Take 0.3g of the above-mentioned particles and disperse them in 10wt% PVA solution, and coat a film on the glass surface. After testing, the transmittances of visible light and near-infrared are 50% and 25% respectively.
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