Water-soluble insecticide with amitraz and method for preparing water-soluble insecticide
A formamidine, water-soluble technology, applied in the field of water-soluble insecticides and their preparation, can solve problems such as hidden safety hazards, large environmental pollution, high residues, etc., achieve production and user safety, improve insecticidal effect, increase significant effect
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Embodiment 1
[0027] A water-soluble insecticide containing amitraz, preferably comprising the following components in mass percentage: amitraz 12.75%,
[0028] Co-solvent 76%, quaternary ammonium salt 6.25%, synergist 5%. The preparation method of the above-mentioned water-soluble insecticide containing amitraz, the steps are:
[0029] Solvent sample 1: Mix amitraz and co-solvent and stir for 20 minutes, then add quaternary ammonium salt and synergist into the stirring tank and stir for 20 minutes, and then discharge to obtain the finished product.
[0030] Reagents and medicines used in the examples are commercially available routine products, in the following examples:
[0031] Decomposition rate calculation formula: Decomposition rate% = (content before storage - content after thermal storage or normal temperature storage) / content before storage × 100%
[0032] The content before storage is the content of the original drug detected when the sample is prepared for storage (54±2°C) fo...
Embodiment 2
[0045] Solvent sample 2: Weigh 12.75kg of amitraz and 66kg of co-solvent, mix and stir for 20 minutes, then add 6.25kg of quaternary ammonium salt and 15kg of synergist into the stirring tank and stir for 20 minutes, and the material is discharged to obtain 100kg of this method Li example of water-soluble insecticides.
[0046] Control sample 1: Commercially available amitraz solution (content of 12.5%, amitraz solution with xylene as solvent, diluted with water to form a milky white emulsion.)
[0047] For the above samples, the determination of the content before storage, the stability test at room temperature and the heat storage test were carried out at the same time. The heat storage samples were placed in an oven at a temperature of 54±2°C for 14 days, and the samples at room temperature were placed for 12 months and 18 respectively. month and 24 months. Use gas chromatography to measure the content of amitraz in the samples before storage, heat storage samples and norm...
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