Superhydrophobic coating containing hollow glass beads and preparation method thereof
A technology of hollow glass microspheres and super-hydrophobic coating, applied in coatings, polyurea/polyurethane coatings, etc., can solve the problems of cumbersome preparation process of super-hydrophobic coating and inability to achieve large-scale application.
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Embodiment 1
[0019] (1) Modification of hollow glass microspheres: 1.8 g of n-octyltriethoxysilane was dissolved in a mixed solution of ethanol-deionized water (the mass fraction of ethanol was 95%), and the temperature was raised to 60° C. after stirring evenly. Add 18.0 g of hollow glass microspheres and continue to stir and react for 4 hours, then dry to obtain surface hydrophobized hollow glass microspheres.
[0020] (2) Preparation of brushing solution: 1. Prepare polyurethane solution according to the mass ratio of polyurethane elastomer and organic solvent 1:6; 2. Prepare polyvinylidene fluoride according to the mass ratio of polyvinylidene fluoride and N-methylpyrrolidone 1:20 Vinyl fluoride solution; 3. Weigh the polyurethane solution and polyvinylidene fluoride solution according to the mass ratio of polyurethane elastomer and polyvinylidene fluoride 6:3 and magnetically stir to obtain a polymer mixed solution A; 4. According to the modified hollow glass micro The mass ratio of t...
Embodiment 2
[0023] (1) Modification of hollow glass microspheres: Dissolve 1.5 g of n-octyltriethoxysilane in a mixed solution of ethanol-deionized water (ethanol mass fraction is 85%), stir evenly and heat up to 60°C. Add 15.0 g of hollow glass microspheres and continue to stir and react for 4 hours, then dry to obtain surface hydrophobized hollow glass microspheres.
[0024] (2) Preparation of brushing solution: 1. Prepare polyurethane solution according to the mass ratio of polyurethane elastomer and organic solvent 1:5; 2. Prepare polyvinylidene fluoride according to the mass ratio of polyvinylidene fluoride and N-methylpyrrolidone 1:20 Vinyl fluoride solution; 3. Weigh the polyurethane solution and polyvinylidene fluoride solution according to the mass ratio of polyurethane elastomer and polyvinylidene fluoride 6:1 and magnetically stir to obtain a polymer mixed solution A; 4. According to the modified hollow glass micro The mass ratio of the solute (polyurethane elastomer + polyviny...
Embodiment 3
[0027] (1) Modification of hollow glass microspheres: Dissolve 2.0 g of perfluorodecyltriethoxysilane in a mixed solution of ethanol-deionized water (the mass fraction of ethanol is 90%), stir evenly and heat up to 70°C . Add 20.0 g of hollow glass microspheres and continue to stir and react for 3 hours, then dry to obtain surface hydrophobized hollow glass microspheres.
[0028] (2) Preparation of brushing solution: 1. Prepare polyurethane solution according to the mass ratio of polyurethane elastomer and organic solvent 1:7; 2. Prepare polyvinylidene fluoride according to the mass ratio of polyvinylidene fluoride and N-methylpyrrolidone 1:18 Vinyl fluoride solution; 3. Weigh the polyurethane solution and polyvinylidene fluoride solution according to the mass ratio of polyurethane elastomer and polyvinylidene fluoride 6:2 and magnetically stir to obtain a polymer mixed solution A; 4. According to the modified hollow glass micro The mass ratio of the beads to the obtained pol...
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