Method and device for graded recovery of mud and base oil in waste oil-based drilling fluid
An oil-based drilling fluid and base oil technology, which can be used in the preparation of liquid hydrocarbon mixtures, earth-moving drilling and wellbore flushing, etc., and can solve the problems of high-efficiency separation and utilization of difficult oil, low recovery efficiency of oil phase, waste of resources, etc.
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[0063] In an oil-based mud drilling project in a shale gas block in Chongqing, the waste oil-based drilling fluid classification recovery test was carried out according to the method and device of the present invention. The specific operation process and effects are described as follows:
[0064] 1. Physical and chemical properties test of oil-based drilling fluid cuttings samples
[0065] 1) Oil, water and solid three-phase content test
[0066] The oil content of the sample is tested by Soxhlet extractor-infrared spectroscopy, the solid content of the sample is tested by the method of muffle furnace drying and weighing, and the water content of the sample is calculated by subtracting the oil and solid content from the total mass; measured The oil content of the sample is 19.4%, the solid content is 63.1%, and the calculated water content is 17.5%.
[0067] 2) Organic matter component test
[0068] The organic matter spectrum of oil-based drilling fluid cuttings measured by...
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