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Method for regenerating waste gypsum model

A waste gypsum and model technology, applied in the field of gypsum, can solve the problems of long pouring time, shorten the initial and final setting time of gypsum powder, and low strength of gypsum powder, so as to improve the strength, prolong the initial and final setting time, and prolong the initial setting time Effect

Active Publication Date: 2019-01-08
厦门佳浴智能卫浴有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Special attention should be paid to the fact that the waste gypsum model contains a certain amount of sodium sulfate and anhydrous calcium sulfate, which makes the strength of the regenerated gypsum powder low. Among them, sodium sulfate is easy to absorb water and expand, and the pressure generated by water absorption and expansion is easy to make the model cracked. The strength of the gypsum model made of recycled gypsum powder is reduced, and sodium sulfate will also shorten the initial and final setting time of the gypsum powder. The volume of the gypsum model for sanitary ceramics is usually large, and the pouring time is usually relatively long. If the initial setting time is too short, Then the workers do not have time to operate, making it difficult to complete the grouting

Method used

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  • Method for regenerating waste gypsum model

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Effect test

Embodiment 1

[0045] This embodiment provides a method for regenerating waste gypsum models. The collected waste gypsum models are smashed and sorted, and impurities and other non-gypsum items are removed first, and then the residue on the waste gypsum model is removed with a brush or a spatula. After crushing, pass the 60-mesh sieve to obtain coarse waste gypsum particles and transfer them to a stirring tank. Add water equivalent to 4 times the weight of the waste gypsum coarse particles and stir for 1.5 hours at 40°C. Centrifuge the filter while it is hot, discard the filtrate, add 4 times the mass of 10% hydrogen peroxide to the filter residue, stir for 1.5 hours, discard the filtrate after filtering, transfer the filter residue to the sedimentation tank, add water equivalent to 3 times the weight of the filter residue, and adjust the pH to 5.0. Let stand for 12 hours, remove the supernatant liquid, take the lower layer of sediment and place it in an autoclave, autoclave at a temperature o...

Embodiment 2

[0047] This embodiment provides a method for regenerating waste gypsum models. The collected waste gypsum models are smashed and sorted, and impurities and other non-gypsum items are removed first, and then the residue on the waste gypsum model is removed with a brush or a spatula. After crushing, pass 80 mesh sieve to obtain coarse waste gypsum particles and transfer them to a stirring tank. Add water equivalent to 5 times the weight of waste gypsum coarse particles and stir at 55°C for 1.0 hour. Centrifuge the filter while it is hot, discard the filtrate, add 5 times the mass of 10% hydrogen peroxide to the filter residue, stir for 2 hours, discard the filtrate after filtration, transfer the filter residue to the sedimentation tank, add water equivalent to 2 times the weight of the filter residue, and adjust the pH to 4. Let stand for 6 hours, remove the supernatant liquid, take the lower layer of sediment and place it in an autoclave, autoclave at a temperature of 120°C and a...

Embodiment 3

[0049] This embodiment provides a method for regenerating waste gypsum models. The collected waste gypsum models are smashed and sorted, and impurities and other non-gypsum items are removed first, and then the residue on the waste gypsum model is removed with a brush or a spatula. After crushing, pass the 60-mesh sieve to obtain coarse waste gypsum particles and transfer them to a stirring tank. Add water equivalent to 3 times the weight of the waste gypsum coarse particles and stir at 35°C for 2 hours. Centrifuge the filter while it is hot, discard the filtrate, add 4 times the weight of 5% hydrogen peroxide to the filter residue, stir for 1 hour, discard the filtrate after filtration, transfer the filter residue to the sedimentation tank, add water equivalent to 4 times the weight of the filter residue, and adjust the pH to 6. Let stand for 18 hours, remove the supernatant liquid, take the lower layer of sediment and place it in an autoclave, autoclave at a temperature of 130...

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Abstract

The invention relates to a method for regenerating a waste gypsum model, and belongs to the field of gypsum. The method comprises the following steps: (1) crushing: crushing the waste gypsum model, and sieving with a sieve of 60-80 mesh to obtain coarse waste gypsum particles; (2) primary purification: adding water into the waste gypsum granules, stirring, and filtering to obtain filter residue A;(3) secondary purification: adding hydrogen peroxide into the filter residue A, stirring, and filtering to obtain filter residue B; (4) tertiary purification: adding water into the filter residue B,adjusting a pH value to 4-6, standing still, and removing supernatant to obtain underlying sediment; (5) autoclaving and drying: autoclaving the underlying sediment, and drying to obtain a drying material; and (6) grinding: mixing the drying material with polyacrylamide for grinding. By adopting the method provided by the invention, impurities in the waste gypsum model can be effectively removed,and the gypsum powder obtained with the regeneration method has relatively high strength when used for preparing the gypsum model.

Description

Technical field [0001] The invention relates to the field of gypsum, in particular to a regeneration method of waste gypsum models. Background technique [0002] Sanitary ceramic products are important supplies in people's lives. One of the main molding methods for the production of sanitary ceramics is grouting, and most of the grouting molding is done in plaster models. Gypsum models are usually used dozens of times before they can be reused and become scrap gypsum models. The production of household porcelain also has a large amount of scrap gypsum models scrapped. According to statistics, every year domestic waste gypsum models only used to make ceramic products are as high as several million tons. At present, the use of waste gypsum models is mainly used by cement companies as part of the raw materials, but the amount of use is limited. Therefore, many waste plaster models in ceramic production areas have become garbage that is not easy to handle. [0003] The main compon...

Claims

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Application Information

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IPC IPC(8): C04B11/26
CPCC04B11/262
Inventor 李小满
Owner 厦门佳浴智能卫浴有限公司
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