Phosphate Laser Neodymium Glass
A phosphate and neodymium glass technology, applied in the field of laser neodymium glass, can solve the problem of difficulty in meeting the requirements of high-power laser devices, and achieve the effects of small photoelastic coefficient, moderate stimulated emission cross section, and high fluorescence lifetime
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[0063] The preparation method of phosphate laser neodymium glass of the present invention comprises the following steps:
[0064] ① Select the glass formula and weigh each raw material;
[0065] ② Fully mix the raw materials evenly to form a mixture;
[0066] ③The temperature of the silicon carbide melting furnace is raised to 1100-1150°C, and the mixture is evenly added to the ceramic material tank in the silicon carbide melting furnace at 20-25Kg / h;
[0067] ④Introduce O into the ceramic material tank 2 +CC1 4 Mixed gas, the air flow is 1-2L / min;
[0068] ⑤ After stopping the ventilation, inject the molten glass into the platinum crucible, and clarify the molten glass at 1200-1250°C for 3-4 hours;
[0069] ⑥ Mechanically stir the molten glass at 1050-1100°C for 2-4 hours;
[0070] ⑦ Pour the prepared glass liquid into a graphite mold for finalization, annealing and cooling.
[0071] Next, the performance and testing method of the phosphate laser neodymium glass of the ...
Embodiment
[0116] Embodiments 1-20 of the present invention are shown in Table 1-2. The composition (mol percent) and photoelastic coefficient B (10 -12 / Pa), stimulated emission cross section σ(10 -20 cm 2 ), fluorescence lifetime τ (μs), acid resistance stability (D A ) and air bubbles. It should be noted that the following examples are merely examples for better understanding of the present invention, and do not limit the present invention in any way.
[0117] Table 1
[0118]
[0119] Table 2
[0120]
[0121] The glass of the above-mentioned embodiment 9 is processed into a 1cm thick sample, and its absorption spectrum is tested with a spectrophotometer to obtain the required absorption spectrum curve for its stimulated emission cross-section test calculation, such as Figure 5 shown.
[0122] The glass of the above-mentioned embodiment 9 is processed into a sample with a thickness of 1mm, and its fluorescence spectrum is measured with a fluorescence spectrometer to obtai...
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