Ferroferric oxide/single-wall carbon nano-angle composite electrode material and preparation method thereof
A single-wall carbon nano-horn and ferric oxide technology, which is applied in the fields of hybrid capacitor electrodes, hybrid/electric double-layer capacitor manufacturing, nanotechnology, etc. Effects of Capacitive Performance
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[0048] The preparation of described SWCNH-COOH is:
[0049] Disperse SWCNH into nitric acid solution, heat and reflux at 100-120°C for 12-24 hours, centrifuge the reaction solution after the reaction is completed, wash and filter repeatedly with deionized water until the filtrate becomes neutral, then vacuum at 80-90°C Dry to obtain SWCNH-COOH, and then disperse SWCNH-COOH in ethylene glycol to form a 0.5-1.0 mg / mL SWCNH-COOH dispersion.
[0050] The SWCNH-COOH and Fe 3 o 4 The nanocomposite of is:
[0051] A. Add 1.35g of FeCl to 100mL of SWCNH-COOH / EG dispersion 3 ·6H 2 O and 0.5g of cetyltrimethylammonium bromide, magnetically stirred at 50-60°C for 2-5h;
[0052] B. After the mixture is evenly dispersed, transfer the obtained mixed solution to the reaction kettle, and then place it at 180°C for constant temperature reaction for 12-18 hours;
[0053] C. After the reaction is completed, cool to room temperature, open the reaction kettle, centrifuge the composite, wash ...
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